methyl (R)-2-((tert-butoxycarbonyl)amino)-3-(3,4-dimethoxyphenyl)propanoate

Base Information

Chemical Name:methyl (R)-2-((tert-butoxycarbonyl)amino)-3-(3,4-dimethoxyphenyl)propanoate
CAS No.:1254365-77-9
Molecular Formula:C₁₇H₂₅NO₆
Molecular Weight:339.389
Hs Code.:

Synonyms:methyl (R)-2-((tert-butoxycarbonyl)amino)-3-(3,4-dimethoxyphenyl)propanoate

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Chemical Property of methyl (R)-2-((tert-butoxycarbonyl)amino)-3-(3,4-dimethoxyphenyl)propanoate

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Technology Process of methyl (R)-2-((tert-butoxycarbonyl)amino)-3-(3,4-dimethoxyphenyl)propanoate

There total 3 articles about methyl (R)-2-((tert-butoxycarbonyl)amino)-3-(3,4-dimethoxyphenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 78392-35-5
2-amino-3-(3,4-dimethoxybenz-1-yl)propanoic acid methyl ester

: 1254365-77-9
methyl (R)-2-((tert-butoxycarbonyl)amino)-3-(3,4-dimethoxyphenyl)propanoate

Guidance literature:: In dichloromethane; at 20 ℃; for 3h;
DOI:10.1002/cmdc.202000153

Reference yield:

: 1254365-42-8
C₁₇H₂₃NO₆

: 1254365-77-9
methyl (R)-2-((tert-butoxycarbonyl)amino)-3-(3,4-dimethoxyphenyl)propanoate

Guidance literature:: With [R,R-RhMe-Duphos]; hydrogen; In methanol; ethyl acetate; for 12h; under 2068.65 Torr;
DOI:10.1016/j.bmcl.2010.08.053

Reference yield:

: 33605-56-0
(R)-2-amino-3-(3,4-dimethoxyphenyl)propanoic acid

: 1254365-77-9
methyl (R)-2-((tert-butoxycarbonyl)amino)-3-(3,4-dimethoxyphenyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / 4 h / Reflux

2: dichloromethane / 3 h / 20 °C

With sulfuric acid; In dichloromethane;
DOI:10.1002/cmdc.202000153