(2(S)-hydroxy-3(R)-amino-4-phenylthiobutanoyl)-L-leucine trifluoroacetate

Base Information

Chemical Name:(2(S)-hydroxy-3(R)-amino-4-phenylthiobutanoyl)-L-leucine trifluoroacetate
CAS No.:114886-76-9
Molecular Formula:C₂HF₃O₂*C₁₆H₂₄N₂O₃S
Molecular Weight:438.468
Hs Code.:

Synonyms:(2(S)-hydroxy-3(R)-amino-4-phenylthiobutanoyl)-L-leucine trifluoroacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2(S)-hydroxy-3(R)-amino-4-phenylthiobutanoyl)-L-leucine trifluoroacetate

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Technology Process of (2(S)-hydroxy-3(R)-amino-4-phenylthiobutanoyl)-L-leucine trifluoroacetate

There total 15 articles about (2(S)-hydroxy-3(R)-amino-4-phenylthiobutanoyl)-L-leucine trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 114886-89-4
(S)-2-((2S,3R)-3-tert-Butoxycarbonylamino-2-hydroxy-4-phenyl-thiobutyrylamino)-4-methyl-pentanoic acid

: 76-05-1
trifluoroacetic acid

: 114886-76-9
(2(S)-hydroxy-3(R)-amino-4-phenylthiobutanoyl)-L-leucine trifluoroacetate

Guidance literature:: With hydrogenchloride; In 1,4-dioxane;
DOI:10.1021/jm00119a022

Reference yield:

: 114886-74-7
-L-leucine methyl ester

: 114886-76-9
(2(S)-hydroxy-3(R)-amino-4-phenylthiobutanoyl)-L-leucine trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / aq. NaOH

2: 72 percent / HCl / dioxane

With hydrogenchloride; sodium hydroxide; In 1,4-dioxane;
DOI:10.1021/jm00119a022

Reference yield:

: 114886-73-6
-L-leucine methyl ester

: 114886-76-9
(2(S)-hydroxy-3(R)-amino-4-phenylthiobutanoyl)-L-leucine trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / Lawesson's reagent / benzene / 2 h / Heating

2: 94 percent / aq. NaOH

3: 72 percent / HCl / dioxane

With Lawessons reagent; hydrogenchloride; sodium hydroxide; In 1,4-dioxane; benzene;
DOI:10.1021/jm00119a022