<α-aspartyl<8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthin-4.2-yl>>-L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine amide trifluoroacetate

Base Information

Chemical Name:<α-aspartyl<8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthin-4.2-yl>>-L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine amide trifluoroacetate
CAS No.:119129-85-0
Molecular Formula:C₂HF₃O₂*C₅₆H₇₅N₁₃O₁₁S
Molecular Weight:1252.38
Hs Code.:

<α-aspartyl<8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthin-4.2-yl>>-L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine amide trifluoroacetate

Synonyms:<α-aspartyl<8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthin-4.2-yl>>-L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine amide trifluoroacetate

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Chemical Property of <α-aspartyl<8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthin-4.2-yl>>-L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine amide trifluoroacetate

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Technology Process of <α-aspartyl<8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthin-4.2-yl>>-L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine amide trifluoroacetate

There total 3 articles about <α-aspartyl<8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthin-4.2-yl>>-L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine amide trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96865-92-8
xanthine amine congener

: 119129-85-0
<α-aspartyl<8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthin-4.2-yl>>-L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine amide trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / dimethylformamide

2: H₂ / 10percent Pd/C / dimethylformamide

3: 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride (EDAC), 1-hydroxybenzotriazole (HOBt) / dimethylformamide / 0.25 h

4: thiophenol

With hydrogen; benzotriazol-1-ol; thiophenol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1021/jm00391a046

Reference yield:

: 108744-21-4
N^α-(tert-butyloxycarbonyl)-α-L-aspartyl-8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthine β-benzyl ester

: 119129-85-0
<α-aspartyl<8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthin-4.2-yl>>-L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine amide trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10percent Pd/C / dimethylformamide

2: 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride (EDAC), 1-hydroxybenzotriazole (HOBt) / dimethylformamide / 0.25 h

3: thiophenol

With hydrogen; benzotriazol-1-ol; thiophenol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1021/jm00391a046

Reference yield:

: 108744-22-5
(S)-3-tert-Butoxycarbonylamino-N-(2-{2-[4-(2,6-dioxo-1,3-dipropyl-2,3,6,7-tetrahydro-1H-purin-8-yl)-phenoxy]-acetylamino}-ethyl)-succinamic acid

: 119129-85-0
<α-aspartyl<8-<4-<<<<(aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthin-4.2-yl>>-L-phenylalanyl-L-phenylalanylglycyl-L-leucyl-L-methionine amide trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride (EDAC), 1-hydroxybenzotriazole (HOBt) / dimethylformamide / 0.25 h

2: thiophenol

With benzotriazol-1-ol; thiophenol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;
DOI:10.1021/jm00391a046