dimethyl(phenyl){(1E,2E)-1-[1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentylidene]hept-2-enyl}silane

Base Information

Chemical Name:dimethyl(phenyl){(1E,2E)-1-[1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentylidene]hept-2-enyl}silane
CAS No.:1032477-57-8
Molecular Formula:C₂₆H₄₃BO₂Si
Molecular Weight:426.523
Hs Code.:

Synonyms:dimethyl(phenyl){(1E,2E)-1-[1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentylidene]hept-2-enyl}silane

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Chemical Property of dimethyl(phenyl){(1E,2E)-1-[1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentylidene]hept-2-enyl}silane

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Technology Process of dimethyl(phenyl){(1E,2E)-1-[1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentylidene]hept-2-enyl}silane

There total 2 articles about dimethyl(phenyl){(1E,2E)-1-[1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentylidene]hept-2-enyl}silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 16336-82-6
(E)-5-dodecen-7-yne

: 185990-03-8
dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane

: 1032477-57-8
dimethyl(phenyl){(1E,2E)-1-[1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentylidene]hept-2-enyl}silane

Guidance literature:: dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane; With palladium(II) acetylacetonate; diisobutylaluminium hydride; triethylphosphine; In cyclohexane; toluene; at -35 - 20 ℃; Inert atmosphere;

(E)-5-dodecen-7-yne; In cyclohexane; toluene; at 80 ℃; for 22h;
DOI:10.1021/ol800768x

Reference yield:

: 16336-82-6
(E)-5-dodecen-7-yne

: 185990-03-8
dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane

: 1032477-58-9
[(1E,3E)-1-butyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)octa-1,3-dienyl](dimethyl)phenylsilane

: 1032477-57-8
dimethyl(phenyl){(1E,2E)-1-[1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pentylidene]hept-2-enyl}silane

Guidance literature:: dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane; With bis(acetylacetonate)nickel(II); diisobutylaluminium hydride; triethylphosphine; In cyclohexane; toluene; at -35 - 20 ℃; Inert atmosphere;

(E)-5-dodecen-7-yne; In cyclohexane; toluene; at 80 ℃; for 44h;
DOI:10.1021/ol800768x