(ethoxycarbonyl)methylcobalt tricarbonyl(PPh)3

Base Information

• Chemical Name: (ethoxycarbonyl)methylcobalt tricarbonyl(PPh)3
• CAS No.: 79170-71-1
• Molecular Formula: C₂₅H₂₂CoO₅P
• Molecular Weight: 492.414

Synonyms:(ethoxycarbonyl)methylcobalt tricarbonyl(PPh)3

Chemical Property of (ethoxycarbonyl)methylcobalt tricarbonyl(PPh)3

Chemical Property:

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Technology Process of (ethoxycarbonyl)methylcobalt tricarbonyl(PPh)3

There total 2 articles about (ethoxycarbonyl)methylcobalt tricarbonyl(PPh)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

EtOOCCH2Co(CO)4 + triphenylphosphine (603-35-0) → (ethoxycarbonyl)methylcobalt tricarbonyl(PPh)3 (79170-71-1)

Guidance literature:

In n-heptane; byproducts: CO; Kinetics;

DOI:10.1021/ja00289a019

Reference yield: 77.0%

Co2(CO)5(CHCO2Et)(PPh3)2 → [Co(CO)2(PPh3)]x + (ethoxycarbonyl)methylcobalt tricarbonyl(PPh)3 (79170-71-1)

Guidance literature:

In dichloromethane; (Ar) soln. Co complex in CH2Cl2 was refluxed for 15 min; ppt. was filtered and washed with CH2Cl2 - (Co(CO)3(PPh3))x, filtrate was chromd. on silica (CH2Cl2);

DOI:10.1021/om100480v

upstream raw materials:

triphenylphosphine

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