Technology Process of C18H16NOP
There total 4 articles about C18H16NOP which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
ethanol;
at 20 ℃;
for 24h;
under 15001.5 Torr;
Autoclave;
DOI:10.1002/ejoc.201100380
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
1.2: 1 h / -78 °C / Inert atmosphere
2.1: triethylamine / diethyl ether / 16 h / 20 °C / Inert atmosphere
3.1: palladium 10% on activated carbon; hydrogen / ethanol / 24 h / 20 °C / 15001.5 Torr / Autoclave
With
palladium 10% on activated carbon; hydrogen; triethylamine; lithium diisopropyl amide;
In
tetrahydrofuran; diethyl ether; ethanol;
DOI:10.1002/ejoc.201100380
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / diethyl ether / 16 h / 20 °C / Inert atmosphere
2: palladium 10% on activated carbon; hydrogen / ethanol / 24 h / 20 °C / 15001.5 Torr / Autoclave
With
palladium 10% on activated carbon; hydrogen; triethylamine;
In
diethyl ether; ethanol;
DOI:10.1002/ejoc.201100380