2,9-bis(4-(3-methoxyphenyl)-2,3,5,6-tetramethylphenyl)-1,10-phenanthroline

Base Information

Chemical Name:2,9-bis(4-(3-methoxyphenyl)-2,3,5,6-tetramethylphenyl)-1,10-phenanthroline
CAS No.:204195-53-9
Molecular Formula:C₄₆H₄₄N₂O₂
Molecular Weight:656.868
Hs Code.:

Synonyms:2,9-bis(4-(3-methoxyphenyl)-2,3,5,6-tetramethylphenyl)-1,10-phenanthroline

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Chemical Property of 2,9-bis(4-(3-methoxyphenyl)-2,3,5,6-tetramethylphenyl)-1,10-phenanthroline

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Technology Process of 2,9-bis(4-(3-methoxyphenyl)-2,3,5,6-tetramethylphenyl)-1,10-phenanthroline

There total 4 articles about 2,9-bis(4-(3-methoxyphenyl)-2,3,5,6-tetramethylphenyl)-1,10-phenanthroline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 10365-98-7,1107579-37-2
3-methoxyphenylboronic acid

: 204195-48-2
2,9-bis(4-bromo-2,3,5,6-tetramethylphenyl)-[1,10]phenanthroline

: 204195-53-9
2,9-bis(4-(3-methoxyphenyl)-2,3,5,6-tetramethylphenyl)-1,10-phenanthroline

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; toluene; at 80 - 90 ℃; for 26h;
DOI:10.1021/ol025885t

Reference yield:

: 66-71-7
1,10-Phenanthroline

: 204195-53-9
2,9-bis(4-(3-methoxyphenyl)-2,3,5,6-tetramethylphenyl)-1,10-phenanthroline

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi / 20 °C

1.2: 70 percent / MnO₂

2.1: n-BuLi / 20 °C

2.2: 51 percent / MnO₂

3.1: 93 percent / aq.Na₂CO₃ / Pd(PPh₃)4 / toluene; methanol / 26 h / 80 - 90 °C

With n-butyllithium; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; toluene;
DOI:10.1021/ol025885t

Reference yield:

: 1646-54-4
1,4-dibromodurene

: 204195-53-9
2,9-bis(4-(3-methoxyphenyl)-2,3,5,6-tetramethylphenyl)-1,10-phenanthroline

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi / 20 °C

1.2: 70 percent / MnO₂

2.1: n-BuLi / 20 °C

2.2: 51 percent / MnO₂

3.1: 93 percent / aq.Na₂CO₃ / Pd(PPh₃)4 / toluene; methanol / 26 h / 80 - 90 °C

With n-butyllithium; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; toluene;
DOI:10.1021/ol025885t