3,6-Bis-(4-nitro-phenyl)-2,5-bis-(4-phenyl-pent-4-enyl)-[1,4,2,5]dioxadiazinane

Base Information

Chemical Name:3,6-Bis-(4-nitro-phenyl)-2,5-bis-(4-phenyl-pent-4-enyl)-[1,4,2,5]dioxadiazinane
CAS No.:103723-22-4
Molecular Formula:C₃₆H₃₆N₄O₆
Molecular Weight:620.705
Hs Code.:

Synonyms:3,6-Bis-(4-nitro-phenyl)-2,5-bis-(4-phenyl-pent-4-enyl)-[1,4,2,5]dioxadiazinane

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Chemical Property of 3,6-Bis-(4-nitro-phenyl)-2,5-bis-(4-phenyl-pent-4-enyl)-[1,4,2,5]dioxadiazinane

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Technology Process of 3,6-Bis-(4-nitro-phenyl)-2,5-bis-(4-phenyl-pent-4-enyl)-[1,4,2,5]dioxadiazinane

There total 4 articles about 3,6-Bis-(4-nitro-phenyl)-2,5-bis-(4-phenyl-pent-4-enyl)-[1,4,2,5]dioxadiazinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 555-16-8
4-nitrobenzaldehdye

: 73737-71-0
N-(4-phenyl-4-pentenyl)hydroxylamine

: 103723-22-4
3,6-Bis-(4-nitro-phenyl)-2,5-bis-(4-phenyl-pent-4-enyl)-[1,4,2,5]dioxadiazinane

Guidance literature:: With 4 A molecular sieve; In toluene; for 12h; Ambient temperature;
DOI:10.1016/S0040-4020(01)96703-1

Reference yield:

: 73737-63-0
4-phenyl-4-pentenaloxime

: 103723-22-4
3,6-Bis-(4-nitro-phenyl)-2,5-bis-(4-phenyl-pent-4-enyl)-[1,4,2,5]dioxadiazinane

Guidance literature:: Multi-step reaction with 2 steps

1: 379 mg / NaBH₃CN, 6N HCl / methanol / 2 h / -40 - -20 °C / pH= 3

2: 72 percent / 4 Angstroem Molecular sieves / toluene / 12 h / Ambient temperature

With hydrogenchloride; 4 A molecular sieve; sodium cyanoborohydride; In methanol; toluene;
DOI:10.1016/S0040-4020(01)96703-1

Reference yield:

: 103722-91-4
4,4,6-Trimethyl-2-(3-phenyl-but-3-enyl)-[1,3]oxazinane

: 103723-22-4
3,6-Bis-(4-nitro-phenyl)-2,5-bis-(4-phenyl-pent-4-enyl)-[1,4,2,5]dioxadiazinane

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / NaOAc, NH₂OH*HCl / Ambient temperature

2: 379 mg / NaBH₃CN, 6N HCl / methanol / 2 h / -40 - -20 °C / pH= 3

3: 72 percent / 4 Angstroem Molecular sieves / toluene / 12 h / Ambient temperature

With hydrogenchloride; 4 A molecular sieve; hydroxylamine hydrochloride; sodium acetate; sodium cyanoborohydride; In methanol; toluene;
DOI:10.1016/S0040-4020(01)96703-1