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Technology Process of C103H161Cl3O24Si3

C103H161Cl3O24Si3

Base Information
  • Chemical Name:C103H161Cl3O24Si3
  • CAS No.:537041-16-0
  • Molecular Formula:C103H161Cl3O24Si3
  • Molecular Weight:1974.01
  • Hs Code.:
C<sub>103</sub>H<sub>161</sub>Cl<sub>3</sub>O<sub>24</sub>Si<sub>3</sub>

Synonyms:C103H161Cl3O24Si3

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Technology Process of C103H161Cl3O24Si3

There total 1 articles about C103H161Cl3O24Si3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

C<sub>51</sub>H<sub>85</sub>Cl<sub>3</sub>O<sub>15</sub>Si<sub>2</sub>
218799-04-3

C51H85Cl3O15Si2

(2R,4S,5S,6R)-4-(t-butyldimethylsiloxy)-6-(4-(triphenylphosphonium)-butyl)-2-methoxy-2-[[4,5-(R,R)-bis-(p-methoxybenzyloxy)-3-(R)-methyl-6-(R)-(2-methylallyl)-tetrahydropyran-2-(R)-yl]-((S)-p-methoxybenzyloxy)-methyl]-5-methyl-tetrahydropyran iodide

(2R,4S,5S,6R)-4-(t-butyldimethylsiloxy)-6-(4-(triphenylphosphonium)-butyl)-2-methoxy-2-[[4,5-(R,R)-bis-(p-methoxybenzyloxy)-3-(R)-methyl-6-(R)-(2-methylallyl)-tetrahydropyran-2-(R)-yl]-((S)-p-methoxybenzyloxy)-methyl]-5-methyl-tetrahydropyran iodide

C<sub>103</sub>H<sub>161</sub>Cl<sub>3</sub>O<sub>24</sub>Si<sub>3</sub>
537041-16-0

C103H161Cl3O24Si3

Guidance literature:
(2R,4S,5S,6R)-4-(t-butyldimethylsiloxy)-6-(4-(triphenylphosphonium)-butyl)-2-methoxy-2-[[4,5-(R,R)-bis-(p-methoxybenzyloxy)-3-(R)-methyl-6-(R)-(2-methylallyl)-tetrahydropyran-2-(R)-yl]-((S)-p-methoxybenzyloxy)-methyl]-5-methyl-tetrahydropyran iodide; With N,N,N,N,N,N-hexamethylphosphoric triamide; calcium hydride; In tetrahydrofuran; at 20 ℃; for 2h;
With lithium hexamethyldisilazane; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 ℃; for 0.166667h;
C51H85Cl3O15Si2; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at 20 ℃; for 0.666667h;
DOI:10.1039/b504151a
upstream raw materials:

C51H85Cl3O15Si2

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