C₄₅H₅₈O₅Si

Base Information

Chemical Name:C₄₅H₅₈O₅Si
CAS No.:1028432-64-5
Molecular Formula:C₄₅H₅₈O₅Si
Molecular Weight:707.038
Hs Code.:

C<sub>45</sub>H<sub>58</sub>O<sub>5</sub>Si

Synonyms:C₄₅H₅₈O₅Si

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Chemical Property of C₄₅H₅₈O₅Si

Chemical Property:

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Technology Process of C₄₅H₅₈O₅Si

There total 16 articles about C₄₅H₅₈O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1028432-63-4
C₄₆H₆₀O₅SSi

: 75-24-1
trimethylaluminum

: 1028432-64-5
C₄₅H₅₈O₅Si

Guidance literature:: C₄₆H₆₀O₅SSi; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 ℃; for 2h; Inert atmosphere;

trimethylaluminum; In hexane; dichloromethane; at -78 - 0 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol800685c

Reference yield:

: 908865-92-9
(2S,3S)-6-(tert-Butyl-diphenyl-silanyloxy)-3-(4-methoxy-benzyloxy)-2-methyl-hexan-1-ol

: 1028432-64-5
C₄₅H₅₈O₅Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0.75 h / 20 °C

2.1: tert.-butyl lithium; 9-methoxy-9-BBN / tetrahydrofuran; diethyl ether; hexane; pentane / 1.17 h / -78 - 20 °C

2.2: 50 °C

3.1: 2,3-Dimethyl-2-butene; dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

3.2: 0 - 20 °C

4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 20 °C / Molecular sieve

5.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 °C / pH 7 / aq. phosphate buffer

6.1: zinc trifluoromethanesulfonate / dichloromethane / 12 h / 20 °C

7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / -78 °C

7.2: -78 - 0 °C

With 1H-imidazole; tetrapropylammonium perruthennate; 2,3-Dimethyl-2-butene; dimethylsulfide borane complex; iodine; tert.-butyl lithium; zinc trifluoromethanesulfonate; 4-methylmorpholine N-oxide; 9-methoxy-9-BBN; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; pentane; 2.2: Suzuki-Miyaura coupling;
DOI:10.1002/chem.201101437

Reference yield:

: 1028432-61-2
C₅₂H₆₄O₆Si

: 1028432-64-5
C₄₅H₅₈O₅Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: 2,3-Dimethyl-2-butene; dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

1.2: 0 - 20 °C

2.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 20 °C / Molecular sieve

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 °C / pH 7 / aq. phosphate buffer

4.1: zinc trifluoromethanesulfonate / dichloromethane / 12 h / 20 °C

5.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / -78 °C

5.2: -78 - 0 °C

With tetrapropylammonium perruthennate; 2,3-Dimethyl-2-butene; dimethylsulfide borane complex; zinc trifluoromethanesulfonate; 4-methylmorpholine N-oxide; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201101437