2-((2-((4-methoxyphenyl)amino)-3-oxo-3,4-dihydroquinoxalin-6-yl)carbamoyl)benzoic acid

Base Information

Chemical Name:2-((2-((4-methoxyphenyl)amino)-3-oxo-3,4-dihydroquinoxalin-6-yl)carbamoyl)benzoic acid
CAS No.:1627523-02-7
Molecular Formula:C₂₃H₁₈N₄O₅
Molecular Weight:430.42
Hs Code.:

Synonyms:2-((2-((4-methoxyphenyl)amino)-3-oxo-3,4-dihydroquinoxalin-6-yl)carbamoyl)benzoic acid

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Chemical Property of 2-((2-((4-methoxyphenyl)amino)-3-oxo-3,4-dihydroquinoxalin-6-yl)carbamoyl)benzoic acid

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Technology Process of 2-((2-((4-methoxyphenyl)amino)-3-oxo-3,4-dihydroquinoxalin-6-yl)carbamoyl)benzoic acid

There total 8 articles about 2-((2-((4-methoxyphenyl)amino)-3-oxo-3,4-dihydroquinoxalin-6-yl)carbamoyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 85-44-9
phthalic anhydride

: 1627522-94-4
7-amino-3-((4-methoxyphenyl)amino)quinoxalin-2(1H)-one

: 1627523-02-7
2-((2-((4-methoxyphenyl)amino)-3-oxo-3,4-dihydroquinoxalin-6-yl)carbamoyl)benzoic acid

Guidance literature:: With acetic acid; at 20 ℃; for 48h;
DOI:10.1016/j.bioorg.2014.05.010

Reference yield:

: 1627522-93-3
3-((4-methoxyphenyl)amino)-7-nitroquinoxalin-2(1H)-one

: 1627523-02-7
2-((2-((4-methoxyphenyl)amino)-3-oxo-3,4-dihydroquinoxalin-6-yl)carbamoyl)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; palladium 10% on activated carbon / tetrahydrofuran; methanol / 24 h / 40 °C

2: acetic acid / 48 h / 20 °C

With palladium 10% on activated carbon; hydrogen; acetic acid; In tetrahydrofuran; methanol;
DOI:10.1016/j.bioorg.2014.05.010

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 1627523-02-7
2-((2-((4-methoxyphenyl)amino)-3-oxo-3,4-dihydroquinoxalin-6-yl)carbamoyl)benzoic acid

Guidance literature:: Multi-step reaction with 7 steps

1: hydrogenchloride / water / 2 h / Reflux

2: potassium nitrate; sulfuric acid / 20 °C

3: trichlorophosphate / 6 h / Reflux

4: isopropyl alcohol / 20 °C

5: hydrogenchloride / water / 50 °C

6: hydrogen; palladium 10% on activated carbon / tetrahydrofuran; methanol / 24 h / 40 °C

7: acetic acid / 48 h / 20 °C

With hydrogenchloride; sulfuric acid; palladium 10% on activated carbon; hydrogen; acetic acid; potassium nitrate; trichlorophosphate; In tetrahydrofuran; methanol; water; isopropyl alcohol;
DOI:10.1016/j.bioorg.2014.05.010