(1R,2S,3R,4R)-4-[(tert-butyldiphenylsilyloxy)methyl]-2,3-isopropylidenedioxy-1-(4-phenyl-1H-1,2,3-triazol-1-yl)cyclopentane

Base Information

Chemical Name:(1R,2S,3R,4R)-4-[(tert-butyldiphenylsilyloxy)methyl]-2,3-isopropylidenedioxy-1-(4-phenyl-1H-1,2,3-triazol-1-yl)cyclopentane
CAS No.:1161113-42-3
Molecular Formula:C₃₃H₃₉N₃O₃Si
Molecular Weight:553.776
Hs Code.:

Synonyms:(1R,2S,3R,4R)-4-[(tert-butyldiphenylsilyloxy)methyl]-2,3-isopropylidenedioxy-1-(4-phenyl-1H-1,2,3-triazol-1-yl)cyclopentane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S,3R,4R)-4-[(tert-butyldiphenylsilyloxy)methyl]-2,3-isopropylidenedioxy-1-(4-phenyl-1H-1,2,3-triazol-1-yl)cyclopentane

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Technology Process of (1R,2S,3R,4R)-4-[(tert-butyldiphenylsilyloxy)methyl]-2,3-isopropylidenedioxy-1-(4-phenyl-1H-1,2,3-triazol-1-yl)cyclopentane

There total 1 articles about (1R,2S,3R,4R)-4-[(tert-butyldiphenylsilyloxy)methyl]-2,3-isopropylidenedioxy-1-(4-phenyl-1H-1,2,3-triazol-1-yl)cyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 112543-78-9
(1R,2R,3S,4R)-4-azido-1-<((tert-butyldiphenylsilyl)oxy)methyl>-2,3-(isopropylidenedioxy)cyclopentane

: 536-74-3
phenylacetylene

: 1161113-42-3
(1R,2S,3R,4R)-4-[(tert-butyldiphenylsilyloxy)methyl]-2,3-isopropylidenedioxy-1-(4-phenyl-1H-1,2,3-triazol-1-yl)cyclopentane

Guidance literature:: With copper; copper(II) sulfate; In water; tert-butyl alcohol; at 125 ℃; for 0.0833333h; Microwave irradiation;
DOI:10.1002/ejoc.200801124

Reference yield: 86.0%

: 1161113-42-3
(1R,2S,3R,4R)-4-[(tert-butyldiphenylsilyloxy)methyl]-2,3-isopropylidenedioxy-1-(4-phenyl-1H-1,2,3-triazol-1-yl)cyclopentane

: 1161113-48-9
(1R,2S,3R,4R)-2,3-dihydroxy-4-(hydroxymethyl)-1-[4-phenyl-1H-1,2,3-triazol-1-yl]cyclopentane

Guidance literature:: (1R,2S,3R,4R)-4-[(tert-butyldiphenylsilyloxy)methyl]-2,3-isopropylidenedioxy-1-(4-phenyl-1H-1,2,3-triazol-1-yl)cyclopentane; With trifluoroacetic acid; In water; at 20 ℃;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1002/ejoc.200801124