C₂₂H₃₆O₃

Base Information

Chemical Name:C₂₂H₃₆O₃
CAS No.:1359296-17-5
Molecular Formula:C₂₂H₃₆O₃
Molecular Weight:348.526
Hs Code.:

C<sub>22</sub>H<sub>36</sub>O<sub>3</sub>

Synonyms:C₂₂H₃₆O₃

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Chemical Property of C₂₂H₃₆O₃

Chemical Property:

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Technology Process of C₂₂H₃₆O₃

There total 6 articles about C₂₂H₃₆O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1341216-67-8
(1R,4R,6R)-6-methyl-4-(10-phenyldecyl)-3,7-dioxabicyclo[4.1.0]heptan-2-one

: 1359296-17-5
C₂₂H₃₆O₃

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1055/s-0030-1260959

Reference yield:

: 1341216-66-7
(1R,4R,6R)-6-methyl-4-(10-phenyldecyl)-3,7-dioxabicyclo[4.1.0]heptan-2-one

: 1359296-17-5
C₂₂H₃₆O₃

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / toluene / 0.5 h / -78 °C / Inert atmosphere

2: sodium tetrahydroborate / ethanol / 4 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; diisobutylaluminium hydride; In ethanol; toluene;
DOI:10.1055/s-0030-1260959

Reference yield:

: (9-phenylnonyl)magnesium bromide

: 1359296-17-5
C₂₂H₃₆O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: copper(l) cyanide / tetrahydrofuran / 2 h / -78 °C / Inert atmosphere

1.2: 4 h / 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran / 0.33 h / -90 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

3.2: 4 h / 20 °C / Inert atmosphere

4.1: dihydrogen peroxide; sodium hydroxide / methanol; water / 0 - 20 °C / Inert atmosphere

5.1: diisobutylaluminium hydride / toluene / 0.5 h / -78 °C / Inert atmosphere

6.1: sodium tetrahydroborate / ethanol / 4 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; n-butyllithium; dihydrogen peroxide; copper(l) cyanide; diisobutylaluminium hydride; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; water; toluene;
DOI:10.1055/s-0030-1260959