N-[1-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-1-phenyl-meth-(Z)-ylidene]-benzamide

Base Information

• Chemical Name: N-[1-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-1-phenyl-meth-(Z)-ylidene]-benzamide
• CAS No.: 188484-83-5
• Molecular Formula: C₂₄H₂₇NO₂
• Molecular Weight: 361.484

Synonyms:N-[1-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-1-phenyl-meth-(Z)-ylidene]-benzamide

Chemical Property of N-[1-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-1-phenyl-meth-(Z)-ylidene]-benzamide

Chemical Property:

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Technology Process of N-[1-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-1-phenyl-meth-(Z)-ylidene]-benzamide

There total 2 articles about N-[1-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-1-phenyl-meth-(Z)-ylidene]-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

Geraniol (106-24-1) + N-Benzoylbenzimidsaeure-isopropylester (99028-37-2) → N-[1-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-1-phenyl-meth-(Z)-ylidene]-benzamide (188484-83-5)

Guidance literature:

In benzene; at 80 ℃;

DOI:10.1021/jo962129q

Reference yield:

N-benzoylbenzamide (614-28-8) → N-[1-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-1-phenyl-meth-(Z)-ylidene]-benzamide (188484-83-5)

Guidance literature:

Multi-step reaction with 2 steps

1: DEAD, Ph₃P / tetrahydrofuran / 1.) 0 deg C, 1 h, 2.) 0 deg C to room temperature, 2 h

2: 84 percent / benzene / 80 °C

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; benzene;

DOI:10.1021/jo962129q

Reference yield: 50.0%

N-[1-((E)-3,7-Dimethyl-octa-2,6-dienyloxy)-1-phenyl-meth-(Z)-ylidene]-benzamide (188484-83-5) → N-(1,5-dimethyl-1-ethenyl-4-hexenyl)dibenzamide

Guidance literature:

With dichloro bis(acetonitrile) palladium(II); In toluene; for 6h; Ambient temperature;

DOI:10.1021/jo962129q

upstream raw materials:

Geraniol

N-Benzoylbenzimidsaeure-isopropylester

N-benzoylbenzamide

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