4-O-Benzoylphloracetophenone 2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside)

Base Information

• Chemical Name: 4-O-Benzoylphloracetophenone 2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside)
• CAS No.: 130471-79-3
• Molecular Formula: C₂₉H₃₀O₁₄
• Molecular Weight: 602.549

Synonyms:4-O-Benzoylphloracetophenone 2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside)

Chemical Property of 4-O-Benzoylphloracetophenone 2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside)

Chemical Property:

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Technology Process of 4-O-Benzoylphloracetophenone 2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside)

There total 1 articles about 4-O-Benzoylphloracetophenone 2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.2%

ο-Benzoyloxy-phloracetophenon (130471-75-9) + 2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl chloride (572-10-1,4451-35-8,4451-36-9,14227-52-2,14227-87-3,14227-88-4,14257-40-0,17081-03-7,19186-60-8,57237-01-1,65982-17-4,65982-18-5,65982-19-6,66966-08-3,144299-57-0) → 4-O-Benzoylphloracetophenone 2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside) (130471-79-3)

Guidance literature:

With mercury(II) cyanide; In nitromethane; Heating;

Reference yield: 60.7%

4-O-Benzoylphloracetophenone 2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside) (130471-79-3) → Phloracetophenone 2-O-α-D-mannopyranoside (130605-63-9)

Guidance literature:

With sodium methylate; In methanol; for 6h; Heating;

Reference yield: 40.8%

4-O-Benzoylphloracetophenone 2-O-(2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside) (130471-79-3) → 2,4,4',6-Tetrahydroxychalcone 2'-O-α-D-mannopyranoside (4547-85-7,72843-28-8,114612-67-8,121545-97-9,130549-92-7,138665-97-1,20565-42-8,26107-98-2,28757-26-8)

Guidance literature:

With potassium hydroxide; In ethanol; Ambient temperature;

upstream raw materials:

ο-Benzoyloxy-phloracetophenon

2,3,4,6-tetra-O-acetyl-α-D-mannopyranosyl chloride

Downstream raw materials:

Phloracetophenone 2-O-α-D-mannopyranoside

2,4,4',6-Tetrahydroxychalcone 2'-O-α-D-mannopyranoside

2',4,4'-6'-Tetrahydroxydihydrochalcone 2'-O-α-D-mannopyranoside

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