17,18-Seco-7-O-(2-methoxyaethoxy)methyl-18,18O-didehydro-17-desoxa-17-(cytochalasin-D)saeure

Base Information

Chemical Name:17,18-Seco-7-O-(2-methoxyaethoxy)methyl-18,18O-didehydro-17-desoxa-17-(cytochalasin-D)saeure
CAS No.:83071-53-8
Molecular Formula:C₃₄H₄₅NO₉
Molecular Weight:611.733
Hs Code.:

Synonyms:17,18-Seco-7-O-(2-methoxyaethoxy)methyl-18,18O-didehydro-17-desoxa-17-(cytochalasin-D)saeure

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Chemical Property of 17,18-Seco-7-O-(2-methoxyaethoxy)methyl-18,18O-didehydro-17-desoxa-17-(cytochalasin-D)saeure

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Technology Process of 17,18-Seco-7-O-(2-methoxyaethoxy)methyl-18,18O-didehydro-17-desoxa-17-(cytochalasin-D)saeure

There total 4 articles about 17,18-Seco-7-O-(2-methoxyaethoxy)methyl-18,18O-didehydro-17-desoxa-17-(cytochalasin-D)saeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 83071-52-7
17,18-Seco-7-O-(2-methoxyaethoxy)methyl-18,18O-didehydrocytochalasin D

: 83071-53-8
17,18-Seco-7-O-(2-methoxyaethoxy)methyl-18,18O-didehydro-17-desoxa-17-(cytochalasin-D)saeure

Guidance literature:: With jones reagent; In water; acetone; at 0 ℃; for 0.5h;
DOI:10.1002/hlca.19820650210

Reference yield:

: 22144-77-0
cytochalasin D

: 83071-53-8
17,18-Seco-7-O-(2-methoxyaethoxy)methyl-18,18O-didehydro-17-desoxa-17-(cytochalasin-D)saeure

Guidance literature:: Multi-step reaction with 4 steps

1: acetonitrile / 24 h / 80 °C

2: 60 percent / NaBH₄ / dioxane; H₂O / 2 h / Ambient temperature

3: 41 percent / HIO₄ / dioxane; H₂O / 0.75 h / Ambient temperature

4: 20 percent / Jones reagent / acetone; H₂O / 0.5 h / 0 °C

With sodium tetrahydroborate; jones reagent; periodic acid; In 1,4-dioxane; water; acetone; acetonitrile;
DOI:10.1002/hlca.19820650210

Reference yield:

: 83095-38-9
7-O-(2-Methoxyaethoxy)methyl-17,17O-dihydrocytochalasin D

: 83071-53-8
17,18-Seco-7-O-(2-methoxyaethoxy)methyl-18,18O-didehydro-17-desoxa-17-(cytochalasin-D)saeure

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / HIO₄ / dioxane; H₂O / 0.75 h / Ambient temperature

2: 20 percent / Jones reagent / acetone; H₂O / 0.5 h / 0 °C

With jones reagent; periodic acid; In 1,4-dioxane; water; acetone;
DOI:10.1002/hlca.19820650210