Monoacetyl-filicinsaeure (2-Acetyl-3.5-Dihydroxy-6.6-dimethyl-cyclohexadien-(2.4)-on)

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Chemical Name:Monoacetyl-filicinsaeure (2-Acetyl-3.5-Dihydroxy-6.6-dimethyl-cyclohexadien-(2.4)-on)
CAS No.:18110-56-0
Molecular Formula:C₁₀H₁₂O₄
Molecular Weight:196.203
Hs Code.:

Synonyms:Monoacetyl-filicinsaeure (2-Acetyl-3.5-Dihydroxy-6.6-dimethyl-cyclohexadien-(2.4)-on)

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Chemical Property of Monoacetyl-filicinsaeure (2-Acetyl-3.5-Dihydroxy-6.6-dimethyl-cyclohexadien-(2.4)-on)

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Technology Process of Monoacetyl-filicinsaeure (2-Acetyl-3.5-Dihydroxy-6.6-dimethyl-cyclohexadien-(2.4)-on)

There total 1 articles about Monoacetyl-filicinsaeure (2-Acetyl-3.5-Dihydroxy-6.6-dimethyl-cyclohexadien-(2.4)-on) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 167960-42-1
2,4-Diacetyl-3,5-dihydroxy-6,6-dimethyl-cyclohexa-2,4-dienone

: 18110-56-0
Monoacetyl-filicinsaeure (2-Acetyl-3.5-Dihydroxy-6.6-dimethyl-cyclohexadien-(2.4)-on)

Guidance literature:: With sulfuric acid; at 80 ℃; for 0.25h;
DOI:10.1246/cl.1995.625

Reference yield: 53.0%

: 18110-56-0
Monoacetyl-filicinsaeure (2-Acetyl-3.5-Dihydroxy-6.6-dimethyl-cyclohexadien-(2.4)-on)

: 298-12-4
Glyoxilic acid

: 160564-04-5
(5-Acetyl-2,4-dihydroxy-3,3-dimethyl-6-oxo-cyclohexa-1,4-dienyl)-(5-acetyl-2,6-dihydroxy-3,3-dimethyl-4-oxo-cyclohexa-1,5-dienyl)-acetic acid

Guidance literature:: With sodium hydroxide; at 0 ℃; for 0.25h;
DOI:10.1246/cl.1995.625

Reference yield:

: 18110-56-0
Monoacetyl-filicinsaeure (2-Acetyl-3.5-Dihydroxy-6.6-dimethyl-cyclohexadien-(2.4)-on)

: (5-Acetyl-2,4-dihydroxy-3,3-dimethyl-6-oxo-cyclohexa-1,4-dienyl)-(5-acetyl-2,6-dihydroxy-3,3-dimethyl-4-oxo-cyclohexa-1,5-dienyl)-acetic acid 2-(4-bromo-phenyl)-2-oxo-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / 0.5percent aq NaOH / 0.25 h / 0 °C

2: 72 percent / NaH / dimethylsulfoxide

With sodium hydroxide; sodium hydride; In dimethyl sulfoxide;
DOI:10.1246/cl.1995.625