(4R,5R)-4-(p-Methoxybenzyl)-2,2-dimethyldioxlan-4,5-dicarbonsaeure-dimethylester

Base Information

Chemical Name:(4R,5R)-4-(p-Methoxybenzyl)-2,2-dimethyldioxlan-4,5-dicarbonsaeure-dimethylester
CAS No.:79917-84-3
Molecular Formula:C₁₇H₂₂O₇
Molecular Weight:338.357
Hs Code.:

Synonyms:(4R,5R)-4-(p-Methoxybenzyl)-2,2-dimethyldioxlan-4,5-dicarbonsaeure-dimethylester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4R,5R)-4-(p-Methoxybenzyl)-2,2-dimethyldioxlan-4,5-dicarbonsaeure-dimethylester

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Technology Process of (4R,5R)-4-(p-Methoxybenzyl)-2,2-dimethyldioxlan-4,5-dicarbonsaeure-dimethylester

There total 2 articles about (4R,5R)-4-(p-Methoxybenzyl)-2,2-dimethyldioxlan-4,5-dicarbonsaeure-dimethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 37031-29-1
(-)-dimethy-2,3-O-isopropylidene-L-tartrate

: 2746-25-0
p-Methoxybenzyl bromide

: 79917-84-3
(4R,5R)-4-(p-Methoxybenzyl)-2,2-dimethyldioxlan-4,5-dicarbonsaeure-dimethylester

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide; In tetrahydrofuran; hexane; at -5 ℃;
DOI:10.1002/hlca.19870700426

Reference yield:

: 37031-29-1
(-)-dimethy-2,3-O-isopropylidene-L-tartrate

: 2746-25-0
p-Methoxybenzyl bromide

: 79980-62-4
(4S,5R)-4-(4-Methoxy-benzyl)-2,2-dimethyl-[1,3]dioxolane-4,5-dicarboxylic acid dimethyl ester

: 79917-84-3
(4R,5R)-4-(p-Methoxybenzyl)-2,2-dimethyldioxlan-4,5-dicarbonsaeure-dimethylester

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide; In tetrahydrofuran; hexane; Yield given. Yields of byproduct given. Title compound not separated from byproducts; -78 deg C -> -5 deg C;
DOI:10.1002/hlca.19870700426