p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-1-thio-α-D-mannopyranoside
CAS No.:1357000-52-2
Molecular Formula:C₃₄H₅₁NO₁₄S
Molecular Weight:729.843
Hs Code.:

Synonyms:p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-1-thio-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-1-thio-α-D-mannopyranoside

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Technology Process of p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-1-thio-α-D-mannopyranoside

There total 5 articles about p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1357000-51-1
p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3-O-benzyl-1-thio-α-D-mannopyranoside

: 1357000-52-2
p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-1-thio-α-D-mannopyranoside

Guidance literature:: With chloro-trimethyl-silane; lithium iodide; In chloroform; at 0 - 20 ℃; for 6h;
DOI:10.3987/COM-11-12332

Reference yield:

: 1242660-03-2
3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-2)-D-glucosaminyl-3-O-benzyl-(4,6)-benzylidene-β-D-mannopyranosyl p-octyloxyphenyl sulfoxide

: 1357000-52-2
p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: triphenylphosphine / tetrachloromethane; acetonitrile / 2 h / Reflux

2: hydrazine hydrate / ethanol; water; toluene / 5 h / Reflux

3: pyridine / 5 h

4: acetic acid / tetrahydrofuran; water / 5 h / 55 °C

5: chloro-trimethyl-silane; lithium iodide / chloroform / 6 h / 0 - 20 °C

With pyridine; chloro-trimethyl-silane; hydrazine hydrate; acetic acid; triphenylphosphine; lithium iodide; In tetrahydrofuran; tetrachloromethane; ethanol; chloroform; water; toluene; acetonitrile;
DOI:10.3987/COM-11-12332

Reference yield:

: C₄₆H₅₉NO₁₃S

: 1357000-52-2
p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 5 h

2: acetic acid / tetrahydrofuran; water / 5 h / 55 °C

3: chloro-trimethyl-silane; lithium iodide / chloroform / 6 h / 0 - 20 °C

With pyridine; chloro-trimethyl-silane; acetic acid; lithium iodide; In tetrahydrofuran; chloroform; water;
DOI:10.3987/COM-11-12332