4-bromo-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5-(1H)-one

Base Information

• Chemical Name: 4-bromo-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5-(1H)-one
• CAS No.: 51867-03-9
• Molecular Formula: C₁₈H₁₄BrNO₂
• Molecular Weight: 356.219

Synonyms:4-bromo-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5-(1H)-one

Chemical Property of 4-bromo-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5-(1H)-one

Chemical Property:

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Technology Process of 4-bromo-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5-(1H)-one

There total 7 articles about 4-bromo-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5-(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1-benzoyl-2,2a,3,4-tetrahydro-1H-benz[cd]indol-5-one (132008-45-8,51867-02-8) → 4-bromo-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5-(1H)-one (51867-03-9)

Guidance literature:

With pyridinium hydrobromide perbromide; acetic acid; at 50 ℃; for 0.25h;

DOI:10.1021/jm00358a012

Reference yield:

1-benzoyl-2,2a,3,4-tetrahydro-1H-benz[cd]indol-5-one (132008-45-8,51867-02-8) → 4-bromo-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5-(1H)-one (51867-03-9)

Guidance literature:

With water; acetic acid; at 55 - 60 ℃; Irradiation_.mit Gluehlampenlicht;

DOI:10.1021/ja01594a039

Reference yield:

5-acetoxy-1-benzoyl-1,2,2a,3-tetrahydro-benz[cd]indole (408331-34-0) → 4-bromo-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5-(1H)-one (51867-03-9)

Guidance literature:

With chloroform; bromine;

DOI:10.1021/ja01594a039

upstream raw materials:

5-acetoxy-1-benzoyl-1,2,2a,3-tetrahydro-benz[cd]indole

1-benzoyl-2,2a,3,4-tetrahydro-1H-benz[cd]indol-5-one

Indole-3-propionic acid

3-(1-benzoyl-indolin-3-yl)-propionic acid

Downstream raw materials:

1-benzoyl-4-bromo-1,2,2a,3,4,5-hexahydro-benz[cd]indol-5-ol

4-azido-1-benzoyl-2,2a,3,4-tetrahydrobenzindol-5-(1H)-one

4,5,5a,6,7,8-hexahydro-4-benzoyl-7-methylindol<3,4-fg>benzoxazolin-8-one

methyl 1-benzoyl-1,2,2a,3,4,5-hexahydro-5-oxo-benzindol-4-ylcarbamate

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