4-[6-(3,3-diethoxy-propyl)-cyclohex-1-enyl]-4-nitro-butyric acid methyl ester

Base Information

Chemical Name:4-[6-(3,3-diethoxy-propyl)-cyclohex-1-enyl]-4-nitro-butyric acid methyl ester
CAS No.:863643-19-0
Molecular Formula:C₁₈H₃₁NO₆
Molecular Weight:357.447
Hs Code.:

Synonyms:4-[6-(3,3-diethoxy-propyl)-cyclohex-1-enyl]-4-nitro-butyric acid methyl ester

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Chemical Property of 4-[6-(3,3-diethoxy-propyl)-cyclohex-1-enyl]-4-nitro-butyric acid methyl ester

Chemical Property:

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Technology Process of 4-[6-(3,3-diethoxy-propyl)-cyclohex-1-enyl]-4-nitro-butyric acid methyl ester

There total 4 articles about 4-[6-(3,3-diethoxy-propyl)-cyclohex-1-enyl]-4-nitro-butyric acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 863643-16-7
dithiocarbonic acid S-[2,2-diethoxy-1-(2-oxo-cyclohexylmethyl)-ethyl] ester O-ethyl ester

: 863643-19-0
4-[6-(3,3-diethoxy-propyl)-cyclohex-1-enyl]-4-nitro-butyric acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 70 percent / Bu₃SnH; AIBN / toluene / 1 h / 100 °C

2.1: N,N-dimethylethylenediamine / 12 h / Heating

2.2: 750 mg / Et₃N / acetonitrile / 8 h / Heating

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; N,N`-dimethylethylenediamine; In toluene; 2.2: Michael addition;
DOI:10.1021/ol051196g

Reference yield:

: 3054-95-3
acrylaldehyde diethyl acetal

: 863643-19-0
4-[6-(3,3-diethoxy-propyl)-cyclohex-1-enyl]-4-nitro-butyric acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 61 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

2.1: 70 percent / Bu₃SnH; AIBN / toluene / 1 h / 100 °C

3.1: N,N-dimethylethylenediamine / 12 h / Heating

3.2: 750 mg / Et₃N / acetonitrile / 8 h / Heating

With 2,2'-azobis(isobutyronitrile); dilauryl peroxide; tri-n-butyl-tin hydride; N,N`-dimethylethylenediamine; In 1,2-dichloro-ethane; toluene; 3.2: Michael addition;
DOI:10.1021/ol051196g

Reference yield:

: 82721-86-6
ethyl [(2-oxocyclohexyl)sulfanyl]methanethioate

: 863643-19-0
4-[6-(3,3-diethoxy-propyl)-cyclohex-1-enyl]-4-nitro-butyric acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 61 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

2.1: 70 percent / Bu₃SnH; AIBN / toluene / 1 h / 100 °C

3.1: N,N-dimethylethylenediamine / 12 h / Heating

3.2: 750 mg / Et₃N / acetonitrile / 8 h / Heating

With 2,2'-azobis(isobutyronitrile); dilauryl peroxide; tri-n-butyl-tin hydride; N,N`-dimethylethylenediamine; In 1,2-dichloro-ethane; toluene; 3.2: Michael addition;
DOI:10.1021/ol051196g