allyl 4-(2-{[5-chloro-2-(3,4-difluorophenoxy)pyridin-3-yl]carbonyl}-1-methylhydrazino)benzoate

Base Information

Chemical Name:allyl 4-(2-{[5-chloro-2-(3,4-difluorophenoxy)pyridin-3-yl]carbonyl}-1-methylhydrazino)benzoate
CAS No.:1097194-80-3
Molecular Formula:C₂₃H₁₈ClF₂N₃O₄
Molecular Weight:473.863
Hs Code.:

Synonyms:allyl 4-(2-{[5-chloro-2-(3,4-difluorophenoxy)pyridin-3-yl]carbonyl}-1-methylhydrazino)benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl 4-(2-{[5-chloro-2-(3,4-difluorophenoxy)pyridin-3-yl]carbonyl}-1-methylhydrazino)benzoate

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Technology Process of allyl 4-(2-{[5-chloro-2-(3,4-difluorophenoxy)pyridin-3-yl]carbonyl}-1-methylhydrazino)benzoate

There total 1 articles about allyl 4-(2-{[5-chloro-2-(3,4-difluorophenoxy)pyridin-3-yl]carbonyl}-1-methylhydrazino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1097196-58-1
5-chloro-2-(3,4-difluorophenoxy)nicotinic acid

: allyl 4-(1-methylhydrazino) benzoate hydrochloride

: 1097194-80-3
allyl 4-(2-{[5-chloro-2-(3,4-difluorophenoxy)pyridin-3-yl]carbonyl}-1-methylhydrazino)benzoate

Guidance literature:: With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 72h;

Reference yield:

: 1097194-80-3
allyl 4-(2-{[5-chloro-2-(3,4-difluorophenoxy)pyridin-3-yl]carbonyl}-1-methylhydrazino)benzoate

: 1097194-81-4
4-(2-{[5-chloro-2-(3,4-difluorophenoxy)pyridin-3-yl]carbonyl}-1-methylhydrazino)benzoic acid

Guidance literature:: With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 - 50 ℃; for 48.5h; Cooling with ice;