(3R)-3-azido-(2,4,5-trifluorophenyl)butyric acid dibenzylamine salt

Base Information

Chemical Name:(3R)-3-azido-(2,4,5-trifluorophenyl)butyric acid dibenzylamine salt
CAS No.:1329036-50-1
Molecular Formula:C₁₀H₈F₃N₃O₂*C₁₄H₁₅N
Molecular Weight:456.467
Hs Code.:

Synonyms:(3R)-3-azido-(2,4,5-trifluorophenyl)butyric acid dibenzylamine salt

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Chemical Property of (3R)-3-azido-(2,4,5-trifluorophenyl)butyric acid dibenzylamine salt

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Technology Process of (3R)-3-azido-(2,4,5-trifluorophenyl)butyric acid dibenzylamine salt

There total 7 articles about (3R)-3-azido-(2,4,5-trifluorophenyl)butyric acid dibenzylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1293293-73-8
(3R)-3-azido-4-(2,4,5-trifluorophenyl)-butyric acid

: 103-49-1
dibenzylamine

: 1329036-50-1
(3R)-3-azido-(2,4,5-trifluorophenyl)butyric acid dibenzylamine salt

Guidance literature:: In ethyl acetate; for 0.416667h;

Reference yield:

: 1293293-72-7
(2S)-1-(2-azido-4-pentenyl)-2,4,5-trifluorobenzene

: 1329036-50-1
(3R)-3-azido-(2,4,5-trifluorophenyl)butyric acid dibenzylamine salt

Guidance literature:: Multi-step reaction with 2 steps

1: potassium permanganate / water; acetone / 3 h / -20 - -10 °C

2: ethyl acetate / 0.42 h

With potassium permanganate; In water; ethyl acetate; acetone;

Reference yield:

: 327-52-6
1-bromo-2,4,5-trifluorobenzene

: 1329036-50-1
(3R)-3-azido-(2,4,5-trifluorophenyl)butyric acid dibenzylamine salt

Guidance literature:: Multi-step reaction with 7 steps

1.1: isopropylmagnesium chloride / tetrahydrofuran / 1.17 h / -20 - 3 °C / Inert atmosphere

1.2: 0.5 h / -10 °C / Inert atmosphere

1.3: 2.5 h / -10 - 0 °C / Inert atmosphere

2.1: sodium hydroxide / water; methanol / 0.58 h

3.1: copper(l) iodide / hexane; tetrahydrofuran / 1.5 h / -20 °C / Inert atmosphere

4.1: dmap; triethylamine / ethyl acetate / 0 °C / Inert atmosphere

5.1: sodium azide / N,N-dimethyl-formamide; water / 2 h / 75 °C

6.1: potassium permanganate / water; acetone / 3 h / -20 - -10 °C

7.1: ethyl acetate / 0.42 h

With dmap; potassium permanganate; copper(l) iodide; sodium azide; isopropylmagnesium chloride; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; hexane; water; ethyl acetate; N,N-dimethyl-formamide; acetone;