C₁₃H₉ClN₂O₅

Base Information

• Chemical Name: C₁₃H₉ClN₂O₅
• CAS No.: 1422047-37-7
• Molecular Formula: C₁₃H₉ClN₂O₅
• Molecular Weight: 308.678
• Mol file: 1422047-37-7.mol

Synonyms:C₁₃H₉ClN₂O₅

Chemical Property of C₁₃H₉ClN₂O₅

Chemical Property:

Purity/Quality:

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Technology Process of C₁₃H₉ClN₂O₅

There total 1 articles about C₁₃H₉ClN₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-Chloro-5-nitropyridine-1-oxide (13198-73-7) + 2-(methoxycarbonyl)phenyl magnesium chloride → C13H9ClN2O5 (1422047-37-7)

Guidance literature:

2-Chloro-5-nitropyridine-1-oxide; 2-(methoxycarbonyl)phenyl magnesium chloride; In tetrahydrofuran; at -50 ℃;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; at 20 ℃; for 4h;

DOI:10.1021/jo302511s

Reference yield: 98.0%

1-methyl-piperazine (109-01-3) + C13H9ClN2O5 (1422047-37-7) → C18H20N4O5 (1422047-38-8)

Guidance literature:

With triethylamine; In tetrahydrofuran; Reflux;

DOI:10.1021/jo302511s

upstream raw materials:

2-Chloro-5-nitropyridine-1-oxide

Downstream raw materials:

C₁₈H₂₀N₄O₅

Refernces