Boc-β³hLys(2-Cl-Cbz)-β³hPhe-OBn

Base Information

• Chemical Name: Boc-β³hLys(2-Cl-Cbz)-β³hPhe-OBn
• CAS No.: 1003570-36-2
• Molecular Formula: C₃₇H₄₆ClN₃O₇
• Molecular Weight: 680.241
• Mol file: 1003570-36-2.mol

Synonyms:Boc-β³hLys(2-Cl-Cbz)-β³hPhe-OBn

Chemical Property of Boc-β³hLys(2-Cl-Cbz)-β³hPhe-OBn

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of Boc-β³hLys(2-Cl-Cbz)-β³hPhe-OBn

There total 1 articles about Boc-β³hLys(2-Cl-Cbz)-β³hPhe-OBn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-3-Amino-4-phenyl-butyric acid benzyl ester (140210-06-6) + (S)-3-<<(tert-butoxy)carbonyl>amino>-7-<<(2-chlorobenzyloxy)carbonyl>amino>heptanoic acid (219967-67-6) → Boc-β3hLys(2-Cl-Cbz)-β3hPhe-OBn (1003570-36-2)

Guidance literature:

With 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;

DOI:10.1021/jm070148u

Reference yield:

Boc-β3hLys(2-Cl-Cbz)-β3hPhe-OBn (1003570-36-2) → C22H35N3O5

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 16h; under 750.075 Torr;

DOI:10.1021/jm070148u

Reference yield:

Boc-β3hLys(2-Cl-Cbz)-β3hPhe-OBn (1003570-36-2) → C32H38ClN3O5

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/jm070148u

upstream raw materials:

(S)-3-Amino-4-phenyl-butyric acid benzyl ester

(S)-3-<<(tert-butoxy)carbonyl>amino>-7-<<(2-chlorobenzyloxy)carbonyl>amino>heptanoic acid