Technology Process of Dodecabismuth germanium icosaoxide
There total 3 articles about Dodecabismuth germanium icosaoxide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
melt;
from milled GeO2 powder and bismuth nitrate; mixt. decompd. at 700°C, ground and melted at 1200°C; according to: B. Kusz, K. Trzebiatowski, M. Gazda, L. Murawski, J. Non-Cryst. Solids 328 (2003) 137;
DOI:10.1016/j.jallcom.2004.06.001
- Guidance literature:
-
In
melt;
from milled GeO2 powder and bismuth nitrate; mixt. decompd. at 700°C, ground and melted at 1200°C; according to: B. Kusz, K. Trzebiatowski, M. Gazda, L. Murawski, J. Non-Cryst. Solids 328 (2003) 137;
DOI:10.1016/j.jallcom.2004.06.001
- Guidance literature:
-
In
neat (no solvent);
milled mixt. of powdered GeO2 and Bi(NO3)3 in platinum crucible was decomp. at 1000 K for 1 h, ground again, heated from room temp. to 1500 K, homogenized by mechanical stirring, quenched by pouring onto a steel plate; X-ray diffraction;
DOI:10.1016/S0038-1098(03)00008-5
