C₃₈H₆₂BrIO₄Si₂

Base Information

Chemical Name:C₃₈H₆₂BrIO₄Si₂
CAS No.:1266178-57-7
Molecular Formula:C₃₈H₆₂BrIO₄Si₂
Molecular Weight:845.887
Hs Code.:

C<sub>38</sub>H<sub>62</sub>BrIO<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₈H₆₂BrIO₄Si₂

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Chemical Property of C₃₈H₆₂BrIO₄Si₂

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Technology Process of C₃₈H₆₂BrIO₄Si₂

There total 11 articles about C₃₈H₆₂BrIO₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1266178-54-4
C₃₈H₆₂Br₂O₄Si₂

: 1266178-57-7
C₃₈H₆₂BrIO₄Si₂

Guidance literature:: With sodium iodide; In acetone; for 60h; Inert atmosphere;
DOI:10.1002/anie.201005850

Reference yield:

: C₃₀H₄₆O₃Si₂

: 1266178-57-7
C₃₈H₆₂BrIO₄Si₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: silver nitrate; calcium carbonate / water; acetone / 4 h / Inert atmosphere; Darkness

2.1: N-Bromosuccinimide; water / 48 h / 10 °C / Inert atmosphere; Darkness

3.1: water; sodium hydrogencarbonate / methanol / Inert atmosphere

4.1: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

5.1: trichloroacetic acid / tetrahydrofuran; water / Inert atmosphere

6.1: pyridine; Dess-Martin periodane / dichloromethane / 4 h / 0 °C / Inert atmosphere

7.1: tert.-butyl lithium / diethyl ether; pentane / 0.08 h / -78 °C / Inert atmosphere

7.2: 0.42 h / -78 °C / Inert atmosphere

8.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C / Inert atmosphere

8.2: -78 - 20 °C / Inert atmosphere

9.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 0 - 20 °C / Inert atmosphere

9.2: Inert atmosphere

10.1: carbon tetrabromide; triphenylphosphine / benzene / 0.5 h / 50 °C / Inert atmosphere

11.1: sodium iodide / acetone / 60 h / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; N-Bromosuccinimide; carbon tetrabromide; water; tert.-butyl lithium; sodium hydrogencarbonate; Dess-Martin periodane; silver nitrate; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; calcium carbonate; sodium iodide; lithium hexamethyldisilazane; trichloroacetic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone; pentane; benzene; 6.1: Dess-Martin oxidation;
DOI:10.1002/anie.201005850

Reference yield:

: 1266178-31-7
C₃₀H₄₆O₃Si₂

: 1266178-57-7
C₃₈H₆₂BrIO₄Si₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: N-Bromosuccinimide; water / 48 h / 10 °C / Inert atmosphere; Darkness

2.1: water; sodium hydrogencarbonate / methanol / Inert atmosphere

3.1: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: trichloroacetic acid / tetrahydrofuran; water / Inert atmosphere

5.1: pyridine; Dess-Martin periodane / dichloromethane / 4 h / 0 °C / Inert atmosphere

6.1: tert.-butyl lithium / diethyl ether; pentane / 0.08 h / -78 °C / Inert atmosphere

6.2: 0.42 h / -78 °C / Inert atmosphere

7.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C / Inert atmosphere

7.2: -78 - 20 °C / Inert atmosphere

8.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 0 - 20 °C / Inert atmosphere

8.2: Inert atmosphere

9.1: carbon tetrabromide; triphenylphosphine / benzene / 0.5 h / 50 °C / Inert atmosphere

10.1: sodium iodide / acetone / 60 h / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; N-Bromosuccinimide; carbon tetrabromide; water; tert.-butyl lithium; sodium hydrogencarbonate; Dess-Martin periodane; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; lithium hexamethyldisilazane; trichloroacetic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone; pentane; benzene; 5.1: Dess-Martin oxidation;
DOI:10.1002/anie.201005850