C₂₅H₂₃NO₄

Base Information

Chemical Name:C₂₅H₂₃NO₄
CAS No.:1321594-70-0
Molecular Formula:C₂₅H₂₃NO₄
Molecular Weight:401.462
Hs Code.:

C<sub>25</sub>H<sub>23</sub>NO<sub>4</sub>

Synonyms:C₂₅H₂₃NO₄

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Chemical Property of C₂₅H₂₃NO₄

Chemical Property:

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Technology Process of C₂₅H₂₃NO₄

There total 5 articles about C₂₅H₂₃NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₃₁NO₄Si

: 1321594-70-0
C₂₅H₂₃NO₄

Guidance literature:: C₂₈H₃₁NO₄Si; With methanol; In dichloromethane; for 0.25h;

With potassium carbonate; In diethyl ether; water;

With hydrogenchloride; In diethyl ether; water; pH=2;
DOI:10.1016/j.tet.2011.06.032

Reference yield:

: C₁₃H₂₁NO₂Si

: 1321594-70-0
C₂₅H₂₃NO₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 2 h / 20 °C

2.1: methanol / dichloromethane / 0.25 h

2.3: pH 2

With methanol; In dichloromethane;
DOI:10.1016/j.tet.2011.06.032

Reference yield:

: 122-00-9
para-methylacetophenone

: 1321594-70-0
C₂₅H₂₃NO₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: ammonium hydroxide / ethanol / 4 h / 60 - 65 °C

1.3: Auto-seeded programmed polythermic preferential crystallization; Resolution of racemate

2.1: sodium hydroxide / water / 72 h / Reflux

3.1: dichloromethane / 4 h / Reflux

4.1: dichloromethane / 2 h / 20 °C

5.1: methanol / dichloromethane / 0.25 h

5.3: pH 2

With methanol; ammonium hydroxide; sodium hydroxide; In ethanol; dichloromethane; water; 1.1: Bucherer-Bergs reaction;
DOI:10.1016/j.tet.2011.06.032