5,6-dihydro-6,11-dimethyl-12-(p-toluenesulfonyl)benzo<5,6>cyclohepta<1,2-c>pyridin-6,11-imine

Base Information

Chemical Name:5,6-dihydro-6,11-dimethyl-12-(p-toluenesulfonyl)benzo<5,6>cyclohepta<1,2-c>pyridin-6,11-imine
CAS No.:78142-08-2
Molecular Formula:C₂₃H₂₂N₂O₂S
Molecular Weight:390.506
Hs Code.:

Synonyms:5,6-dihydro-6,11-dimethyl-12-(p-toluenesulfonyl)benzo<5,6>cyclohepta<1,2-c>pyridin-6,11-imine

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Chemical Property of 5,6-dihydro-6,11-dimethyl-12-(p-toluenesulfonyl)benzo<5,6>cyclohepta<1,2-c>pyridin-6,11-imine

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Technology Process of 5,6-dihydro-6,11-dimethyl-12-(p-toluenesulfonyl)benzo<5,6>cyclohepta<1,2-c>pyridin-6,11-imine

There total 4 articles about 5,6-dihydro-6,11-dimethyl-12-(p-toluenesulfonyl)benzo<5,6>cyclohepta<1,2-c>pyridin-6,11-imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78142-07-1
6,11-dimethyl-11-p-toluenesulfonamidobenzo<5,6>cyclohepta<1,2-c>pyridine

: 78142-08-2
5,6-dihydro-6,11-dimethyl-12-(p-toluenesulfonyl)benzo<5,6>cyclohepta<1,2-c>pyridin-6,11-imine

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; for 2h; Heating;
DOI:10.1002/jhet.5570230129

Reference yield:

: 78142-06-0
N-(p-toluenesulfonyl)-6-methylbenzo<5,6>cyclohepta<1,2-c>pyridin-6,11-imine

: 78142-08-2
5,6-dihydro-6,11-dimethyl-12-(p-toluenesulfonyl)benzo<5,6>cyclohepta<1,2-c>pyridin-6,11-imine

Guidance literature:: Multi-step reaction with 2 steps

1: 3.13 g / tetrahydrofuran / 2 h

2: 1.0 g / 50 aq. NaOH / dioxane / 2 h / Heating

With sodium hydroxide; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1002/jhet.5570230129

Reference yield:

: 78142-05-9
6-methylbenzo<5,6>cyclohepta<1,2-c>pyridin-11-imine

: 78142-08-2
5,6-dihydro-6,11-dimethyl-12-(p-toluenesulfonyl)benzo<5,6>cyclohepta<1,2-c>pyridin-6,11-imine

Guidance literature:: Multi-step reaction with 3 steps

1: 5.3 g / pyridine / Ambient temperature; overnight

2: 3.13 g / tetrahydrofuran / 2 h

3: 1.0 g / 50 aq. NaOH / dioxane / 2 h / Heating

With sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; pyridine;
DOI:10.1002/jhet.5570230129