allyl(2-methylallyl)phenylphosphino-borane

Base Information

Chemical Name:allyl(2-methylallyl)phenylphosphino-borane
CAS No.:294183-95-2
Molecular Formula:C₁₃H₂₀BP
Molecular Weight:218.087
Hs Code.:

Synonyms:allyl(2-methylallyl)phenylphosphino-borane

Suppliers and Price of allyl(2-methylallyl)phenylphosphino-borane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of allyl(2-methylallyl)phenylphosphino-borane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of allyl(2-methylallyl)phenylphosphino-borane

There total 1 articles about allyl(2-methylallyl)phenylphosphino-borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: (Rp)-(+)-N-[(1S,2R)-2-hydroxy-1-methylphenylethyl]-N-methyl-P-allylphosphineamine-P-borane

: 5674-01-1
2-methylallylmagnesium chloride

: 294183-95-2
allyl(2-methylallyl)phenylphosphino-borane

Guidance literature:: With hydrogenchloride; In diethyl ether; byproducts: ephedrine chloride; HCl(gas) was bubbled through a soln. borane-complex in Et2O at 0°C until pptn. was complete, stirred for 15 min at room temp., filtered, the solvent was removed, dissolved in Et2O, Mg-compound was added at -78°C, 1.5 h at room temp.; quenched with aq. satd. NH4Cl at -10°C, the organic phase was washed with water, aq. satd. NH4Cl, dried (MgSO4), evapd. under vac., column chromy. (petroleum ether-toluene); as oil;
DOI:10.1039/b306940k

Reference yield: 90.0%

: 294183-95-2
allyl(2-methylallyl)phenylphosphino-borane

: 179989-97-0
1-phenyl-2,5-dihydro-3-methyl-1H-phosphole-1-borane

Guidance literature:: dichloro(tricyclohexylphosphino)(benzylidene)(1,3-dimesityl-4,5-dihydroimidazol-2-ylidene)ruthenium(III); In dichloromethane; 6 mol % catalysts was added to a soln. of phoshane in CH2Cl2, which was boiling under reflux for 26 h (Ar); volatiles were removed, column chromy. on silica gel;
DOI:10.1039/b306940k