N,N-bis{6-[(4-methoxybenzyl)oxy]hexa-2,4-diyn-1-yl}-4-methylbenzenesulfonamide

Base Information

• Chemical Name: N,N-bis{6-[(4-methoxybenzyl)oxy]hexa-2,4-diyn-1-yl}-4-methylbenzenesulfonamide
• CAS No.: 1510816-16-6
• Molecular Formula: C₃₅H₃₃NO₆S
• Molecular Weight: 595.716

Synonyms:N,N-bis{6-[(4-methoxybenzyl)oxy]hexa-2,4-diyn-1-yl}-4-methylbenzenesulfonamide

Chemical Property of N,N-bis{6-[(4-methoxybenzyl)oxy]hexa-2,4-diyn-1-yl}-4-methylbenzenesulfonamide

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Technology Process of N,N-bis{6-[(4-methoxybenzyl)oxy]hexa-2,4-diyn-1-yl}-4-methylbenzenesulfonamide

There total 1 articles about N,N-bis{6-[(4-methoxybenzyl)oxy]hexa-2,4-diyn-1-yl}-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

1-{[(3-bromoprop-2-yn-1-yl)oxy]methyl}-4-methoxybenzene (1115284-86-0) + 4-methyl-N,N-diprop-2-ynylbenzenesulfonamide (18773-54-1) → N,N-bis{6-[(4-methoxybenzyl)oxy]hexa-2,4-diyn-1-yl}-4-methylbenzenesulfonamide (1510816-16-6)

Guidance literature:

With piperidine; copper(l) chloride; at 0 ℃; for 1h;

DOI:10.1021/ol403258c

Reference yield: 77.0%

N,N-bis{6-[(4-methoxybenzyl)oxy]hexa-2,4-diyn-1-yl}-4-methylbenzenesulfonamide (1510816-16-6) → 4,5-dichloro-6-{[(3-methoxybenzyl)oxy]methyl}-7-{3-[(4-methoxybenzyl)oxy]prop-1-yn-1-yl}-2-tosylisoindoline (1510816-03-1)

Guidance literature:

With dilithium tetrachlorocuprate; In tetrahydrofuran; at 68 ℃; for 18h;

DOI:10.1021/ol403258c

Reference yield: 72.0%

N,N-bis{6-[(4-methoxybenzyl)oxy]hexa-2,4-diyn-1-yl}-4-methylbenzenesulfonamide (1510816-16-6) → 1-methoxy-7-{3-[(4-methoxybenzyl)oxy]prop-1-yn-1-yl}-9-tosyl-6,8,9,10-tetrahydro-1H,4H-1,3a-ethenoisochromeno[5,4-ef]isoindole (1510816-05-3)

Guidance literature:

In tetrahydrofuran; at 68 ℃; for 18h;

DOI:10.1021/ol403258c

upstream raw materials:

1-{[(3-bromoprop-2-yn-1-yl)oxy]methyl}-4-methoxybenzene

4-methyl-N,N-diprop-2-ynylbenzenesulfonamide

Downstream raw materials:

4,5-dichloro-6-{[(3-methoxybenzyl)oxy]methyl}-7-{3-[(4-methoxybenzyl)oxy]prop-1-yn-1-yl}-2-tosylisoindoline

1-methoxy-7-{3-[(4-methoxybenzyl)oxy]prop-1-yn-1-yl}-9-tosyl-6,8,9,10-tetrahydro-1H,4H-1,3a-ethenoisochromeno[5,4-ef]isoindole

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