N¹-methyl-N¹-[2-(4-phenylpiperazin-1-yl)ethyl]benzene-1,3-diamine hydrochloride

Base Information

Chemical Name:N¹-methyl-N¹-[2-(4-phenylpiperazin-1-yl)ethyl]benzene-1,3-diamine hydrochloride
CAS No.:1610999-00-2
Molecular Formula:C₁₉H₂₆N₄*ClH
Molecular Weight:346.903
Hs Code.:

N<sup>1</sup>-methyl-N<sup>1</sup>-[2-(4-phenylpiperazin-1-yl)ethyl]benzene-1,3-diamine hydrochloride

Synonyms:N¹-methyl-N¹-[2-(4-phenylpiperazin-1-yl)ethyl]benzene-1,3-diamine hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N¹-methyl-N¹-[2-(4-phenylpiperazin-1-yl)ethyl]benzene-1,3-diamine hydrochloride

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Technology Process of N¹-methyl-N¹-[2-(4-phenylpiperazin-1-yl)ethyl]benzene-1,3-diamine hydrochloride

There total 5 articles about N¹-methyl-N¹-[2-(4-phenylpiperazin-1-yl)ethyl]benzene-1,3-diamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1610998-84-9
N-methyl-3-nitro-N-[2-(4-phenylpiperazin-1-yl)ethyl]aniline hydrochloride

: 1610999-00-2
N¹-methyl-N¹-[2-(4-phenylpiperazin-1-yl)ethyl]benzene-1,3-diamine hydrochloride

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; ethyl acetate; at 20 ℃; for 5h; under 760.051 Torr;
DOI:10.1016/j.ejmech.2014.04.034

Reference yield:

: 1611526-92-1
N-methyl-3-nitro-N-[2-(4-phenylpiperazin-1-yl)ethyl]aniline

: 1610999-00-2
N¹-methyl-N¹-[2-(4-phenylpiperazin-1-yl)ethyl]benzene-1,3-diamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / methanol

2: hydrogen; palladium 10% on activated carbon / ethyl acetate; ethanol / 5 h / 20 °C / 760.05 Torr

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; In methanol; ethanol; ethyl acetate;
DOI:10.1016/j.ejmech.2014.04.034

Reference yield:

: 619-26-1
N-methyl-3-nitroaniline

: 1610999-00-2
N¹-methyl-N¹-[2-(4-phenylpiperazin-1-yl)ethyl]benzene-1,3-diamine hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydrogencarbonate / ethyl acetate; water / 0.33 h / 20 °C / Cooling with ice

2: triethylamine / N,N-dimethyl-formamide / 20 °C

3: diborane / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere; Cooling with ice

4: hydrogenchloride / methanol

5: hydrogen; palladium 10% on activated carbon / ethyl acetate; ethanol / 5 h / 20 °C / 760.05 Torr

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; triethylamine; diborane; In tetrahydrofuran; methanol; ethanol; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.04.034