C₃₁H₃₇NO₅S

Base Information

Chemical Name:C₃₁H₃₇NO₅S
CAS No.:1334124-09-2
Molecular Formula:C₃₁H₃₇NO₅S
Molecular Weight:535.704
Hs Code.:

C<sub>31</sub>H<sub>37</sub>NO<sub>5</sub>S

Synonyms:C₃₁H₃₇NO₅S

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Chemical Property of C₃₁H₃₇NO₅S

Chemical Property:

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Technology Process of C₃₁H₃₇NO₅S

There total 1 articles about C₃₁H₃₇NO₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 107-02-8,25068-14-8
acrolein

: 187324-67-0
(1S,2R)-2-(N-benzyl-N-mesitylenesulfonyl)amino-1-phenyl-1-propyl propionate

: 1334124-09-2
C₃₁H₃₇NO₅S

Guidance literature:: (1S,2R)-2-(N-benzyl-N-mesitylenesulfonyl)amino-1-phenyl-1-propyl propionate; With triethylamine; dicyclohexyl(((trifluoromethyl)sulfonyl)oxy)borane; In dichloromethane; at -78 ℃;

acrolein;
DOI:10.1055/s-0030-1260822

Reference yield: 96.0%

: 1334124-09-2
C₃₁H₃₇NO₅S

: 69739-34-0
t-butyldimethylsiyl triflate

: 1334123-97-5
C₃₇H₅₁NO₅SSi

Guidance literature:: With triethylamine; at 20 ℃; for 1h;
DOI:10.1055/s-0030-1260822

Reference yield:

: 1334124-09-2
C₃₁H₃₇NO₅S

: C₂₂H₂₉Cl₃O₄Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: triethylamine / 1 h / 20 °C

2.1: diisobutylaluminium hydride / -78 - 20 °C

3.1: sodium hydrogencarbonate; Dess-Martin periodane / 20 °C

4.1: triphenylphosphine / 10 h / 0 °C

4.2: -78 - 20 °C

5.1: hydrogenchloride / methanol; water / 20 °C

6.1: N-ethyl-N,N-diisopropylamine

7.1: dimethyllithium cuprate / tetrahydrofuran / 6 h / -78 °C

8.1: hydrogenchloride / methanol; water / 5 h / 60 °C

9.1: water; lithium hydroxide / methanol / 20 °C

10.1: triethylamine / 4 h / 0 °C

11.1: triethylamine / toluene / 20 °C

With hydrogenchloride; water; dimethyllithium cuprate; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium hydroxide; In tetrahydrofuran; methanol; water; toluene; 11.1: Yamaguchi esterification;
DOI:10.1055/s-0030-1260822