bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid methyl ester

Base Information

Chemical Name:bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid methyl ester
CAS No.:714251-15-7
Molecular Formula:C₄₅H₄₅O₈P
Molecular Weight:744.821
Hs Code.:

Synonyms:bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid methyl ester

Suppliers and Price of bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid methyl ester

There total 1 articles about bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 67309-03-9
bis(hydroxymethyl)phosphinic acid O-methyl ester

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 714251-15-7
bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid methyl ester

Guidance literature:: With pyridine; at 20 ℃; for 12h;
DOI:10.1016/S0040-4039(02)01067-5

Reference yield:

: 714251-15-7
bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid methyl ester

: [bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-[(2-cyano-ethoxy)-diisopropylamino-phosphanyloxymethyl]-phosphinic acid 2-(5-methyl-2,6-dioxo-5,6-dihydro-2H-pyrimidin-1-yl)-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 10 h / 100 °C

2: 75 percent / 1-(2-mesitylensulfonyl)-3-nitro-1,2,4-triazole; pyridine / 24 h / 20 °C

3: 33 percent / toluene-4-sulfonic acid / methanol / 0.08 h / 20 °C

4: 60 percent / 2-ethylthio-1H-tetrazole / acetonitrile / 1 h / 20 °C

With pyridine; 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; toluene-4-sulfonic acid; 5-(ethylthio)-1H-tetrazole; In methanol; acetonitrile;
DOI:10.1016/S0040-4039(02)01067-5

Reference yield:

: 714251-15-7
bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid methyl ester

: C₃₉H₅₁N₅O₈P₂

Guidance literature:: Multi-step reaction with 4 steps

1: 10 h / 100 °C

2: 25 percent / triphenylphosphine; carbon tetrachloride; pyridiene / 24 h / 20 °C

3: 30 percent / toluene-4-sulfonic acid / methanol / 0.08 h / 20 °C

4: 50 percent / 2-ethylthio-1H-tetrazole / acetonitrile / 1 h / 20 °C

With pyridine; tetrachloromethane; toluene-4-sulfonic acid; 5-(ethylthio)-1H-tetrazole; triphenylphosphine; In methanol; acetonitrile; 2: Appel reaction;
DOI:10.1016/S0040-4039(02)01067-5