ethyl (E)-2-diethoxyphosphoryl-3-(4-trifluoromethylphenyl)propendithioate

Base Information

• Chemical Name: ethyl (E)-2-diethoxyphosphoryl-3-(4-trifluoromethylphenyl)propendithioate
• CAS No.: 287929-30-0
• Molecular Formula: C₁₆H₂₀F₃O₃PS₂
• Molecular Weight: 412.434
• Mol file: 287929-30-0.mol

Synonyms:ethyl (E)-2-diethoxyphosphoryl-3-(4-trifluoromethylphenyl)propendithioate

Chemical Property of ethyl (E)-2-diethoxyphosphoryl-3-(4-trifluoromethylphenyl)propendithioate

Chemical Property:

Purity/Quality:

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Technology Process of ethyl (E)-2-diethoxyphosphoryl-3-(4-trifluoromethylphenyl)propendithioate

There total 1 articles about ethyl (E)-2-diethoxyphosphoryl-3-(4-trifluoromethylphenyl)propendithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

ethyl 2-(diethoxyphosphoryl)ethanedithioate + 4,4'-((4-(trifluoromethyl)phenyl)methylene)dimorpholine → ethyl (E)-2-diethoxyphosphoryl-3-(4-trifluoromethylphenyl)propendithioate (287929-30-0)

Guidance literature:

With chloroacetic acid; In toluene; at 20 ℃; for 48h;

DOI:10.1016/S0040-4020(00)00297-0

Reference yield:

tert-butyl vinyl ether (926-02-3) + ethyl (E)-2-diethoxyphosphoryl-3-(4-trifluoromethylphenyl)propendithioate (287929-30-0) → trans-2-tert-butoxy-5-diethoxyphosphonyl-3,4-dihydro-6-ethylthio-4-(4-trifluoromethylphenyl)-2H-thiopyran + cis-2-tert-butoxy-5-diethoxyphosphonyl-3,4-dihydro-6-ethylthio-4-(4-trifluoromethylphenyl)-2H-thiopyran

Guidance literature:

at 20 ℃; for 72h; under 8250660 Torr; Further Variations:; Pressures; Temperatures; reaction times; Product distribution;

DOI:10.1016/S0040-4020(00)00297-0