fluoromethyl benzyl sulfide

Base Information

• Chemical Name: fluoromethyl benzyl sulfide
• CAS No.: 2924-74-5
• Molecular Formula: C₈H₉FS
• Molecular Weight: 156.224
• Mol file: 2924-74-5.mol

Synonyms:fluoromethyl benzyl sulfide

Chemical Property of fluoromethyl benzyl sulfide

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of fluoromethyl benzyl sulfide

There total 6 articles about fluoromethyl benzyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

R32 (593-70-4) + phenylmethanethiol (100-53-8) → fluoromethyl benzyl sulfide (2924-74-5)

Guidance literature:

phenylmethanethiol; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

R₃₂; In N,N-dimethyl-formamide; at 70 ℃; for 3h;

DOI:10.1002/adsc.201800136

Reference yield:

[(methylthio)methyl]-benzene (766-92-7) → fluoromethyl benzyl sulfide (2924-74-5) + α-fluoro-α-(methylthio)toluene

Guidance literature:

With diethylamino-sulfur trifluoride; antimony(III) chloride; In dichloromethane; for 1h; Yield given. Yields of byproduct given; Ambient temperature;

DOI:10.1021/jo00067a009

Reference yield:

N-tosyl-S-fluoromethyl-S-phenylsulfoximine + phenylmethanethiol (100-53-8) → fluoromethyl benzyl sulfide (2924-74-5)

Guidance literature:

phenylmethanethiol; With sodium hydride; In dimethyl sulfoxide; at 20 ℃; for 0.5h;

N-tosyl-S-fluoromethyl-S-phenylsulfoximine; In dimethyl sulfoxide; at 80 ℃; for 4h;

DOI:10.1039/c3sc51831k

upstream raw materials:

benzyl chloromethyl sulfide

R₃₂

phenylmethanethiol

[(methylthio)methyl]-benzene

Downstream raw materials:

hydrogen fluoride

benzyl methoxymethyl sulfide