C₂₇H₃₈O₆Si

Base Information

Chemical Name:C₂₇H₃₈O₆Si
CAS No.:1032879-98-3
Molecular Formula:C₂₇H₃₈O₆Si
Molecular Weight:486.681
Hs Code.:

C<sub>27</sub>H<sub>38</sub>O<sub>6</sub>Si

Synonyms:C₂₇H₃₈O₆Si

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Chemical Property of C₂₇H₃₈O₆Si

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Technology Process of C₂₇H₃₈O₆Si

There total 8 articles about C₂₇H₃₈O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1032879-85-8
C₂₇H₃₈O₅Si

: 1032879-98-3
C₂₇H₃₈O₆Si

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In water; tert-butyl alcohol; at -10 - 20 ℃;
DOI:10.1021/ol8008057

Reference yield:

: 1032879-81-4
C₂₇H₃₈O₄Si

: 1032879-98-3
C₂₇H₃₈O₆Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 5 h / 0 - 20 °C

1.2: 2 h / Reflux

2.1: dimethyl sulfoxide; triethylamine; sulfur trioxide pyridine complex / dichloromethane / 2 h / -10 °C

3.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol / 1 h / -10 - 20 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.3987/COM-12-S(N)54

Reference yield:

: 101331-92-4
4-O-(tert-butyldiphenylsilyl)-2,3-O-isopropylidene-L-threose

: 1032879-98-3
C₂₇H₃₈O₆Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: (-)-B-methoxydiisopinocamphenylborane / diethyl ether / 1 h / 0 - 20 °C

1.2: 3 h / -78 °C

2.1: sodium hydride / tetrahydrofuran / 1 h / -10 - 20 °C

2.2: 12 h / 20 °C

3.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 5 h / 0 - 20 °C

3.2: 2 h / Reflux

4.1: dimethyl sulfoxide; triethylamine; sulfur trioxide pyridine complex / dichloromethane / 2 h / -10 °C

5.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol / 1 h / -10 - 20 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; (-)-B-methoxydiisopinocamphenylborane; sulfur trioxide pyridine complex; sodium hydride; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; diethyl ether; dichloromethane; water; tert-butyl alcohol;
DOI:10.3987/COM-12-S(N)54