1'-(4-methoxyphenyl)-<1'-oxy>-<2-<(1,1-dimethylethyl)dimethylsilyl>oxy>ethane

Base Information

Chemical Name:1'-(4-methoxyphenyl)-<1'-oxy>-<2-<(1,1-dimethylethyl)dimethylsilyl>oxy>ethane
CAS No.:166248-68-6
Molecular Formula:C₂₀H₃₄O₄Si
Molecular Weight:366.573
Hs Code.:

1'-(4-methoxyphenyl)-<1'-<tetrhydropyranyl>oxy>-<2-<(1,1-dimethylethyl)dimethylsilyl>oxy>ethane

Synonyms:1'-(4-methoxyphenyl)-<1'-oxy>-<2-<(1,1-dimethylethyl)dimethylsilyl>oxy>ethane

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Chemical Property of 1'-(4-methoxyphenyl)-<1'-oxy>-<2-<(1,1-dimethylethyl)dimethylsilyl>oxy>ethane

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Technology Process of 1'-(4-methoxyphenyl)-<1'-oxy>-<2-<(1,1-dimethylethyl)dimethylsilyl>oxy>ethane

There total 5 articles about 1'-(4-methoxyphenyl)-<1'-oxy>-<2-<(1,1-dimethylethyl)dimethylsilyl>oxy>ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 110-87-2
3,4-dihydro-2H-pyran

: 166248-67-5
1'-(4-methoxyphenyl)-<2'-<(1,1-dimethylethyl)dimethylsilyl>oxy>ethanol

: 166248-68-6
1'-(4-methoxyphenyl)-<1'-oxy>-<2-<(1,1-dimethylethyl)dimethylsilyl>oxy>ethane

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4020(01)89330-3

Reference yield:

: 2'-(1E/Z,3E,5E,7E,9E-dodecapentaenyloxy)-1'-(4-methoxyphenyl)ethanol

: 166248-68-6
1'-(4-methoxyphenyl)-<1'-oxy>-<2-<(1,1-dimethylethyl)dimethylsilyl>oxy>ethane

Guidance literature:: Multi-step reaction with 3 steps

1: 37 percent / H₂O / 5 h

2: 84 percent / imidazole / dimethylformamide / 1 h / Ambient temperature

3: 90 percent / p-TsOH*H₂O / CH₂Cl₂ / Ambient temperature

With 1H-imidazole; toluene-4-sulfonic acid; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)89330-3

Reference yield:

: 58518-78-8
p-methoxyphenacyl acetate

: 166248-68-6
1'-(4-methoxyphenyl)-<1'-oxy>-<2-<(1,1-dimethylethyl)dimethylsilyl>oxy>ethane

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / LiAlH₄ / diethyl ether / 2 h, reflux, 4 h and room t.

2: 84 percent / imidazole / dimethylformamide / 1 h / Ambient temperature

3: 90 percent / p-TsOH*H₂O / CH₂Cl₂ / Ambient temperature

With 1H-imidazole; lithium aluminium tetrahydride; toluene-4-sulfonic acid; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)89330-3