5,7,12,13b,13c,14-hexahydro-1,4,8,11-tetrakis<2-(2-chloro-ethoxy)ethoxy>-13b,13c-diphenyl-6H,13H-5a,6a,12a,13a-tetraazabenz<5,6>azuleno<2,1,8-ija>benzazulene-6,13-dione

Base Information

• Chemical Name: 5,7,12,13b,13c,14-hexahydro-1,4,8,11-tetrakis<2-(2-chloro-ethoxy)ethoxy>-13b,13c-diphenyl-6H,13H-5a,6a,12a,13a-tetraazabenz<5,6>azuleno<2,1,8-ija>benzazulene-6,13-dione
• CAS No.: 118715-67-6
• Molecular Formula: C₄₈H₅₄Cl₄N₄O₁₀
• Molecular Weight: 988.79

Synonyms:5,7,12,13b,13c,14-hexahydro-1,4,8,11-tetrakis<2-(2-chloro-ethoxy)ethoxy>-13b,13c-diphenyl-6H,13H-5a,6a,12a,13a-tetraazabenz<5,6>azuleno<2,1,8-ija>benzazulene-6,13-dione

Chemical Property of 5,7,12,13b,13c,14-hexahydro-1,4,8,11-tetrakis<2-(2-chloro-ethoxy)ethoxy>-13b,13c-diphenyl-6H,13H-5a,6a,12a,13a-tetraazabenz<5,6>azuleno<2,1,8-ija>benzazulene-6,13-dione

Chemical Property:

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• Pictogram(s):  
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Technology Process of 5,7,12,13b,13c,14-hexahydro-1,4,8,11-tetrakis<2-(2-chloro-ethoxy)ethoxy>-13b,13c-diphenyl-6H,13H-5a,6a,12a,13a-tetraazabenz<5,6>azuleno<2,1,8-ija>benzazulene-6,13-dione

There total 6 articles about 5,7,12,13b,13c,14-hexahydro-1,4,8,11-tetrakis<2-(2-chloro-ethoxy)ethoxy>-13b,13c-diphenyl-6H,13H-5a,6a,12a,13a-tetraazabenz<5,6>azuleno<2,1,8-ija>benzazulene-6,13-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

1,6:3,4-bis(2-oxapropylene)tetrahydro-3a,6a-diphenylimidazo[4,5-d]imidazole-2,5(1H,3H)-dione (121619-22-5) + p-bis<2-(2'-chloroethoxy)ethoxy>benzene (93179-57-8) → 5,7,12,13b,13c,14-hexahydro-1,4,8,11-tetrakis<2-(2-chloro-ethoxy)ethoxy>-13b,13c-diphenyl-6H,13H-5a,6a,12a,13a-tetraazabenz<5,6>azuleno<2,1,8-ija>benzazulene-6,13-dione (118715-67-6)

Guidance literature:

With acetic anhydride; trifluoroacetic acid; at 95 ℃; for 0.5h;

DOI:10.1002/recl.19931121207

Reference yield: 39.0%

1,6:3,4-bis(2-oxapropylene)tetrahydro-3a,6a-diphenylimidazo[4,5-d]imidazole-2,5(1H,3H)-dione (121619-22-5) + p-bis<2-(2'-chloroethoxy)ethoxy>benzene (93179-57-8) → 5,7,12,13b,13c,14-hexahydro-1,4,8,11-tetrakis<2-(2-chloro-ethoxy)ethoxy>-13b,13c-diphenyl-6H,13H-5a,6a,12a,13a-tetraazabenz<5,6>azuleno<2,1,8-ija>benzazulene-6,13-dione (118715-67-6) + C44H46Cl4N4O8 + 5,7,12,13b,13c,14-Hexahydro-1(and 11)-(2-chloroethoxy)-4,8,11(and 1)-tris<2-(2-chloroethoxy)ethoxy>-13b,13c-diphenyl-6H,13H-5a,6a,12a,13a-tetraazabenz<5,6>azuleno-<2,1,8-ija>benzazulene-6,13-dione + C44H46Cl4N4O8

Guidance literature:

With acetic anhydride; 1-(2-Chloroethoxy)-4-<2-(2-chloroethoxy)ethoxy>benzene; trifluoroacetic acid; 1.) 95 deg C, 30 min, 2.) 95 deg C, 30 min;

DOI:10.1002/recl.19951140205

Reference yield: 39.0%

1,6:3,4-bis(2-oxapropylene)tetrahydro-3a,6a-diphenylimidazo[4,5-d]imidazole-2,5(1H,3H)-dione (121619-22-5) + 1-(2-Chloroethoxy)-4-<2-(2-chloroethoxy)ethoxy>benzene (165274-91-9) → 5,7,12,13b,13c,14-hexahydro-1,4,8,11-tetrakis<2-(2-chloro-ethoxy)ethoxy>-13b,13c-diphenyl-6H,13H-5a,6a,12a,13a-tetraazabenz<5,6>azuleno<2,1,8-ija>benzazulene-6,13-dione (118715-67-6) + C44H46Cl4N4O8 + 5,7,12,13b,13c,14-Hexahydro-1(and 11)-(2-chloroethoxy)-4,8,11(and 1)-tris<2-(2-chloroethoxy)ethoxy>-13b,13c-diphenyl-6H,13H-5a,6a,12a,13a-tetraazabenz<5,6>azuleno-<2,1,8-ija>benzazulene-6,13-dione + C44H46Cl4N4O8

Guidance literature:

With acetic anhydride; p-bis<2-(2'-chloroethoxy)ethoxy>benzene; trifluoroacetic acid; 1.) 95 deg C, 30 min, 2.) 95 deg C, 30 min;

DOI:10.1002/recl.19951140205

upstream raw materials:

2-(2-chloroethoxy)ethyl tosylate

5,7,12,13b,13c,14-hexahydro-1,4,8,11-tetrahydroxy-13b,13c-diphenyl-6H,13H-5a,6a,12a,13a-tetraazabenz[5,6]azuleno[2,1,8-ija]benz[f]azulene-6,13-dione

1,6:3,4-bis(2-oxapropylene)tetrahydro-3a,6a-diphenylimidazo[4,5-d]imidazole-2,5(1H,3H)-dione

p-bis<2-(2'-chloroethoxy)ethoxy>benzene

Downstream raw materials:

2a,8,9,12,13,14,15,17,18,25,26,29,30,31,32,34,35,38b-octadecahydro-2a,38b-diphenyl-13,30-bis<4-(methoxymethoxy)phenylmethyl>-1H,4H-6,37:20,23-dietheno-2,22:3.21-dimethano-5H,11H,28H,38H-7,10,16,19,24,27,33,36-octaoxa-2,3,4a,13,30,38a-hexaazacyclopent...

C₆₀H₆₂N₄O₁₄

1,3:4,6-bis<3,3':6,6'-bis(1,4,10,13-tetraoxa-7-benzyl-7-azatridecamethylene)-1,2-xylylene>tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione

C₆₈H₆₆N₄O₁₄

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