2-isobutyl-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triyne

Base Information

Chemical Name:2-isobutyl-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triyne
CAS No.:1353055-23-8
Molecular Formula:C₃₇H₄₁N₃O₆S₃
Molecular Weight:719.947
Hs Code.:

Synonyms:2-isobutyl-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triyne

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Chemical Property of 2-isobutyl-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triyne

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Technology Process of 2-isobutyl-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triyne

There total 5 articles about 2-isobutyl-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1079308-71-6
N,N'-bis(4-chloro-2-butynyl)-(4-methylphenyl)sulfonamide

: 1353055-36-3
N,N'-bis[(4-methylphenyl)sulfonyl]-1-isobutyl-2-butyne-1,4-diamine

: 1353055-23-8
2-isobutyl-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triyne

Guidance literature:: With potassium carbonate; In acetonitrile; for 25h; Reflux;
DOI:10.1021/om200927f

Reference yield:

: 1353055-32-9
6-methyl-2-heptyne-1,4-diol

: 1353055-23-8
2-isobutyl-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triyne

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C

2: trifluoroacetic acid / dichloromethane / 9.5 h / 20 °C

3: potassium carbonate / acetonitrile / 25 h / Reflux

With di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; acetonitrile; 1: Mitsunobu reaction;
DOI:10.1021/om200927f

Reference yield:

: 1353055-34-1
N,N'-bis(tertbutyloxycarbonyl)-N,N'-bis[(4-methylphenyl)sulfonyl]-1-isobutyl-2-butyne-1,4-diamine

: 1353055-23-8
2-isobutyl-1,6,11-tris[(4-methylphenyl)sulfonyl]-1,6,11-triazacyclopentadeca-3,8,13-triyne

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 9.5 h / 20 °C

2: potassium carbonate / acetonitrile / 25 h / Reflux

With potassium carbonate; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1021/om200927f