(cholest-5-en-3β-yl)-N-[13-hydroxy-7-(2-nitrophenylsulfonyl)-7-azatridecyl]carbamate

Base Information

Chemical Name:(cholest-5-en-3β-yl)-N-[13-hydroxy-7-(2-nitrophenylsulfonyl)-7-azatridecyl]carbamate
CAS No.:1243558-21-5
Molecular Formula:C₄₆H₇₅N₃O₇S
Molecular Weight:814.183
Hs Code.:

Synonyms:(cholest-5-en-3β-yl)-N-[13-hydroxy-7-(2-nitrophenylsulfonyl)-7-azatridecyl]carbamate

Suppliers and Price of (cholest-5-en-3β-yl)-N-[13-hydroxy-7-(2-nitrophenylsulfonyl)-7-azatridecyl]carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (cholest-5-en-3β-yl)-N-[13-hydroxy-7-(2-nitrophenylsulfonyl)-7-azatridecyl]carbamate

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Technology Process of (cholest-5-en-3β-yl)-N-[13-hydroxy-7-(2-nitrophenylsulfonyl)-7-azatridecyl]carbamate

There total 6 articles about (cholest-5-en-3β-yl)-N-[13-hydroxy-7-(2-nitrophenylsulfonyl)-7-azatridecyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1191385-33-7
6-(cholest-5-ene-3β-yloxycarbamino)hexylbromide

: 1243558-15-7
N-(6-hydroxyhexyl)-2-nitrobenzenesulfonyl amide

: 1243558-21-5
(cholest-5-en-3β-yl)-N-[13-hydroxy-7-(2-nitrophenylsulfonyl)-7-azatridecyl]carbamate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 3h;
DOI:10.1007/s11172-010-0070-y

Reference yield:

: 143723-62-0
(cholest-5-en-3β-yl) N-(4-hydroxyhexyl)carbamate

: 1243558-21-5
(cholest-5-en-3β-yl)-N-[13-hydroxy-7-(2-nitrophenylsulfonyl)-7-azatridecyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: carbon tetrabromide; triphenylphosphine / dichloromethane / 0 - 25 °C

2: caesium carbonate / N,N-dimethyl-formamide / 3 h / 80 °C

With carbon tetrabromide; caesium carbonate; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1007/s11172-010-0070-y

Reference yield:

: 4048-33-3
6-amino-1-hexanol

: 1243558-21-5
(cholest-5-en-3β-yl)-N-[13-hydroxy-7-(2-nitrophenylsulfonyl)-7-azatridecyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 24 h / 4 - 24 °C / Molecular sieve

2: caesium carbonate / N,N-dimethyl-formamide / 3 h / 80 °C

With caesium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1007/s11172-010-0070-y