(R)-N-(3-((5-chloro-2-(2,4-dichlorophenoxy)phenyl)amino)-3-oxopropyl)-2,4-dihydroxy-3,3-dimethylbutanamide

Base Information

Chemical Name:(R)-N-(3-((5-chloro-2-(2,4-dichlorophenoxy)phenyl)amino)-3-oxopropyl)-2,4-dihydroxy-3,3-dimethylbutanamide
CAS No.:1610839-94-5
Molecular Formula:C₂₁H₂₃Cl₃N₂O₅
Molecular Weight:489.783
Hs Code.:

Synonyms:(R)-N-(3-((5-chloro-2-(2,4-dichlorophenoxy)phenyl)amino)-3-oxopropyl)-2,4-dihydroxy-3,3-dimethylbutanamide

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Chemical Property of (R)-N-(3-((5-chloro-2-(2,4-dichlorophenoxy)phenyl)amino)-3-oxopropyl)-2,4-dihydroxy-3,3-dimethylbutanamide

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Technology Process of (R)-N-(3-((5-chloro-2-(2,4-dichlorophenoxy)phenyl)amino)-3-oxopropyl)-2,4-dihydroxy-3,3-dimethylbutanamide

There total 3 articles about (R)-N-(3-((5-chloro-2-(2,4-dichlorophenoxy)phenyl)amino)-3-oxopropyl)-2,4-dihydroxy-3,3-dimethylbutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1610840-01-1
(4R)-N-(3-(5-chloro-2-(2,4-dichlorophenoxy)phenylamino)-3-oxopropyl)-2-(4-methoxyphenyl)-5,5-dimethyl-1,3-dioxane-4-carboxamide

: 1610839-94-5
(R)-N-(3-((5-chloro-2-(2,4-dichlorophenoxy)phenyl)amino)-3-oxopropyl)-2,4-dihydroxy-3,3-dimethylbutanamide

Guidance literature:: With water; acetic acid; at 20 ℃; for 16h;
DOI:10.1016/j.bmc.2014.04.030

Reference yield:

: 79-83-4
pantothenic acid

: 1610839-94-5
(R)-N-(3-((5-chloro-2-(2,4-dichlorophenoxy)phenyl)amino)-3-oxopropyl)-2,4-dihydroxy-3,3-dimethylbutanamide

Guidance literature:: Multi-step reaction with 3 steps

1: camphor-10-sulfonic acid / N,N-dimethyl-formamide / 16 h / 20 °C

2: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 80 °C

3: acetic acid; water / 16 h / 20 °C

With camphor-10-sulfonic acid; water; acetic acid; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2014.04.030

Reference yield:

: 864239-47-4
3-{[(4R)-2-(p-methoxyphenyl)-5,5-dimethyl-1,3-dioxan-4-yl]carbonylamino}propionic acid

: 1610839-94-5
(R)-N-(3-((5-chloro-2-(2,4-dichlorophenoxy)phenyl)amino)-3-oxopropyl)-2,4-dihydroxy-3,3-dimethylbutanamide

Guidance literature:: Multi-step reaction with 2 steps

1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 80 °C

2: acetic acid; water / 16 h / 20 °C

With water; acetic acid; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2014.04.030