[4-({11-[4-(benzyloxycarbonylaminomethyl)benzylcarbamoyl]undecanoylamino}methyl)benzyl]carbamic acid benzyl ester

Base Information

Chemical Name:[4-({11-[4-(benzyloxycarbonylaminomethyl)benzylcarbamoyl]undecanoylamino}methyl)benzyl]carbamic acid benzyl ester
CAS No.:428880-00-6
Molecular Formula:C₄₄H₅₄N₄O₆
Molecular Weight:734.936
Hs Code.:

Synonyms:[4-({11-[4-(benzyloxycarbonylaminomethyl)benzylcarbamoyl]undecanoylamino}methyl)benzyl]carbamic acid benzyl ester

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Chemical Property of [4-({11-[4-(benzyloxycarbonylaminomethyl)benzylcarbamoyl]undecanoylamino}methyl)benzyl]carbamic acid benzyl ester

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Technology Process of [4-({11-[4-(benzyloxycarbonylaminomethyl)benzylcarbamoyl]undecanoylamino}methyl)benzyl]carbamic acid benzyl ester

There total 1 articles about [4-({11-[4-(benzyloxycarbonylaminomethyl)benzylcarbamoyl]undecanoylamino}methyl)benzyl]carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 693-23-2
1,12-dodecanedioic acid

: 164648-85-5
benzyl N-[4-(aminomethyl)benzyl]carbamate

: 428880-00-6
[4-({11-[4-(benzyloxycarbonylaminomethyl)benzylcarbamoyl]undecanoylamino}methyl)benzyl]carbamic acid benzyl ester

Guidance literature:: 1,12-dodecanedioic acid; With chloroformic acid ethyl ester; triethylamine; In 1,4-dioxane; for 0.5h;

benzyl N-[4-(aminomethyl)benzyl]carbamate; In 1,4-dioxane; at 20 ℃; Further stages.;
DOI:10.1021/jm011067f

Reference yield: 100.0%

: 428880-00-6
[4-({11-[4-(benzyloxycarbonylaminomethyl)benzylcarbamoyl]undecanoylamino}methyl)benzyl]carbamic acid benzyl ester

: 428880-01-7
dodecanedioic acid bis(4-aminomethylbenzylamide)

Guidance literature:: With acetic acid; trifluoroacetic acid; for 2h;
DOI:10.1021/jm011067f

Reference yield:

: 428880-00-6
[4-({11-[4-(benzyloxycarbonylaminomethyl)benzylcarbamoyl]undecanoylamino}methyl)benzyl]carbamic acid benzyl ester

: 428880-02-8
dodecanedioic acid bis{4-[(2-methoxybenzylamino)methyl]benzylamide}

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / 30percent HBr; AcOH; CF₃COOH / 2 h

2: methanol / 2 h / Heating

3: NaBH₄ / methanol / 5 h / 20 °C

With sodium tetrahydroborate; acetic acid; trifluoroacetic acid; In methanol;
DOI:10.1021/jm011067f