C₂₃H₂₁N

Base Information

• Chemical Name: C₂₃H₂₁N
• CAS No.: 1443502-05-3
• Molecular Formula: C₂₃H₂₁N
• Molecular Weight: 311.426
• Mol file: 1443502-05-3.mol

Synonyms:C₂₃H₂₁N

Chemical Property of C₂₃H₂₁N

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₃H₂₁N

There total 4 articles about C₂₃H₂₁N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

C20H19NO (1443501-93-6) + allyl bromide (106-95-6) → C23H21N (1443502-05-3)

Guidance literature:

With palladium dichloride; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

DOI:10.1021/jo401013d

Reference yield:

C25H22N2O3S (1443501-86-7) → C23H21N (1443502-05-3)

Guidance literature:

Multi-step reaction with 2 steps

1: magnesium / methanol / 0 - 20 °C

2: palladium dichloride / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With magnesium; palladium dichloride; In methanol; N,N-dimethyl-formamide;

DOI:10.1021/jo401013d

Reference yield:

C21H16N2O3S (1443501-77-6) → C23H21N (1443502-05-3)

Guidance literature:

Multi-step reaction with 3 steps

1: indium; ammonium chloride / tetrahydrofuran; water / 0 - 20 °C

2: magnesium / methanol / 0 - 20 °C

3: palladium dichloride / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With indium; ammonium chloride; magnesium; palladium dichloride; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;

DOI:10.1021/jo401013d

upstream raw materials:

C₂₅H₂₂N₂O₃S

C₂₀H₁₉NO

allyl bromide

C₁₆H₁₃NO