C₁₄H₂₂O₃

Base Information

• Chemical Name: C₁₄H₂₂O₃
• CAS No.: 1315379-05-5
• Molecular Formula: C₁₄H₂₂O₃
• Molecular Weight: 238.327
• Mol file: 1315379-05-5.mol

Synonyms:C₁₄H₂₂O₃

Chemical Property of C₁₄H₂₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₂₂O₃

There total 5 articles about C₁₄H₂₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

C21H26O3 → C14H22O3 (1315379-05-5)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 8h;

DOI:10.1055/s-0030-1260532

Reference yield:

C19H22O2 → C14H22O3 (1315379-05-5)

Guidance literature:

Multi-step reaction with 3 steps

1: trimethylaluminum / hexane / 0.5 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 9 h / 20 °C

3: palladium 10% on activated carbon; hydrogen / ethanol / 8 h / 20 °C

With palladium 10% on activated carbon; hydrogen; trimethylaluminum; N-ethyl-N,N-diisopropylamine; In ethanol; hexane; dichloromethane; 1: Claisen rearrangement;

DOI:10.1055/s-0030-1260532

Reference yield:

C19H22O2 → C14H22O3 (1315379-05-5)

Guidance literature:

Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 9 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / ethanol / 8 h / 20 °C

With palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane;

DOI:10.1055/s-0030-1260532

upstream raw materials:

R-(E)-1-(benzyloxy)pent-3-en-2-ol

3-methyl-phenol

Downstream raw materials:

(S)-curcuphenol

Refernces