Benzoic acid (2S,3R,5R)-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-yl ester

Base Information

Chemical Name:Benzoic acid (2S,3R,5R)-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-yl ester
CAS No.:171036-33-2
Molecular Formula:C₁₃H₁₆O₄
Molecular Weight:236.268
Hs Code.:

Synonyms:Benzoic acid (2S,3R,5R)-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-yl ester

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Chemical Property of Benzoic acid (2S,3R,5R)-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-yl ester

Chemical Property:

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Technology Process of Benzoic acid (2S,3R,5R)-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-yl ester

There total 9 articles about Benzoic acid (2S,3R,5R)-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 582-25-2
Potassium benzoate

: 171036-33-2
Benzoic acid (2S,3R,5R)-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / dimethylformamide / 48 h / 100 °C

2: 1.) trifluoroacetic acid, hydrochloric acid, 2.) sodium borohydride / 1.) water, 4 deg C, 24 h, 2.) methanol, room temperature, 24 h

With hydrogenchloride; sodium tetrahydroborate; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(96)00082-1

Reference yield:

: 153974-01-7
2,5-anhydro-3,6-di-O-methanesulfonyl-L-idose ethylene acetal

: 171036-33-2
Benzoic acid (2S,3R,5R)-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / pyridine / 48 h / 4 °C

2: 58 percent / sodium hydrogensulfide monohydrate / dimethylformamide / 3 h / 90 °C

3: 24 percent / Raney Ni, hydrogen / ethanol / 24 h / Ambient temperature

4: 54 percent / dimethylformamide / 48 h / 100 °C

5: 1.) trifluoroacetic acid, hydrochloric acid, 2.) sodium borohydride / 1.) water, 4 deg C, 24 h, 2.) methanol, room temperature, 24 h

With pyridine; hydrogenchloride; sodium tetrahydroborate; sodium hydrogensulfide; hydrogen; nickel; trifluoroacetic acid; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(96)00082-1

Reference yield:

: 181645-44-3
Methanesulfonic acid (2S,3S,5R)-5-[1,3]dioxolan-2-yl-2-methyl-tetrahydro-furan-3-yl ester

: 171036-33-2
Benzoic acid (2S,3R,5R)-5-hydroxymethyl-2-methyl-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / dimethylformamide / 48 h / 100 °C

2: 1.) trifluoroacetic acid, hydrochloric acid, 2.) sodium borohydride / 1.) water, 4 deg C, 24 h, 2.) methanol, room temperature, 24 h

With hydrogenchloride; sodium tetrahydroborate; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(96)00082-1