2-[4-Benzyloxy-1-methyl-1-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-butyl]-3-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxymethyl)-benzo[1,4]dioxine

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Chemical Name:2-[4-Benzyloxy-1-methyl-1-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-butyl]-3-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxymethyl)-benzo[1,4]dioxine
CAS No.:123845-46-5
Molecular Formula:C₄₃H₆₄O₁₃
Molecular Weight:788.973
Hs Code.:

2-[4-Benzyloxy-1-methyl-1-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-butyl]-3-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxymethyl)-benzo[1,4]dioxine

Synonyms:2-[4-Benzyloxy-1-methyl-1-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-butyl]-3-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxymethyl)-benzo[1,4]dioxine

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Chemical Property of 2-[4-Benzyloxy-1-methyl-1-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-butyl]-3-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxymethyl)-benzo[1,4]dioxine

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Technology Process of 2-[4-Benzyloxy-1-methyl-1-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-butyl]-3-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxymethyl)-benzo[1,4]dioxine

There total 6 articles about 2-[4-Benzyloxy-1-methyl-1-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-butyl]-3-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxymethyl)-benzo[1,4]dioxine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 85539-28-2
2-(2'-(2''-Chloroethoxy)ethoxy)ethyl-2-tetrahydro-2H-pyran

: 123845-42-1
α-methyl-2-<3-(phenylmethoxy)propyl>-benzo-1,4-dioxin-2,3-dimethanol

: 123845-46-5
2-[4-Benzyloxy-1-methyl-1-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-butyl]-3-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxymethyl)-benzo[1,4]dioxine

Guidance literature:: With tetra(n-butyl)ammonium hydrogensulfate; In sodium hydroxide; water; at 35 ℃;
DOI:10.1016/S0040-4039(00)99472-3

Reference yield:

: 1071-73-4
5-Hydroxy-2-pentanone

: 123845-46-5
2-[4-Benzyloxy-1-methyl-1-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-butyl]-3-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxymethyl)-benzo[1,4]dioxine

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutylammonium hydrogen sulfate, benzene / NaOH; H₂O

3: 91 percent / lithium aluminium hydride / diethyl ether / Ambient temperature

4: 70 percent / tetrabutyl-ammonium hydrogen sulfate / NaOH; H₂O / 35 °C

With lithium aluminium tetrahydride; tetra(n-butyl)ammonium hydrogensulfate; benzene; In sodium hydroxide; diethyl ether; water;
DOI:10.1016/S0040-4039(00)99472-3

Reference yield:

: 123845-41-0
3-methyl-3-<3-(phenylmethoxy)propyl>furo<3,4-b><1,4>benzodioxin-1-(3H)-one

: 123845-46-5
2-[4-Benzyloxy-1-methyl-1-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-butyl]-3-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxymethyl)-benzo[1,4]dioxine

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / lithium aluminium hydride / diethyl ether / Ambient temperature

2: 70 percent / tetrabutyl-ammonium hydrogen sulfate / NaOH; H₂O / 35 °C

With lithium aluminium tetrahydride; tetra(n-butyl)ammonium hydrogensulfate; In sodium hydroxide; diethyl ether; water;
DOI:10.1016/S0040-4039(00)99472-3