2--(4'-chloroacetophenone)

Base Information

Chemical Name:2--(4'-chloroacetophenone)
CAS No.:102436-69-1
Molecular Formula:C₁₆H₁₅ClN₂O₃
Molecular Weight:318.76
Hs Code.:

2-<N-methyl-N-(2-nitrobenzyl)amino>-(4'-chloroacetophenone)

Synonyms:2--(4'-chloroacetophenone)

Suppliers and Price of 2--(4'-chloroacetophenone)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2--(4'-chloroacetophenone)

Chemical Property:

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Technology Process of 2--(4'-chloroacetophenone)

There total 1 articles about 2--(4'-chloroacetophenone) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 56222-08-3
(2-nitrobenzyl)methylamine

: 536-38-9
4-chlorobenzoylmethyl bromide

: 102436-69-1
2--(4'-chloroacetophenone)

Guidance literature:: With triethylamine; In diethyl ether; at 18 - 25 ℃; for 4h;
DOI:10.1021/jm00157a012

Reference yield: 70.0%

: 102436-69-1
2--(4'-chloroacetophenone)

: 168412-66-6
N-(2-nitrobenzyl)-2-(methylamino)-1-(4'-chlorophenyl)-1-ethanol

Guidance literature:: With sodium tetrahydroborate; In methanol; water; for 4h; Ambient temperature;
DOI:10.1021/jm00157a012

Reference yield:

: 102436-69-1
2--(4'-chloroacetophenone)

: 89845-16-9
4-(4-chlorophenyl)-8-<(ethoxy-carbonyl)amino>-2-methyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / NaBH₄ / methanol; H₂O / 4 h / Ambient temperature

2: 80 percent / H₂ / Raney nickel / ethanol / 12 h / 760 Torr

3: 34 percent / conc. H₂SO₄ / CH₂Cl₂ / 0.5 h / 6 - 8 °C

4: 46 percent / benzene / 3 h / Heating

With sodium tetrahydroborate; sulfuric acid; hydrogen; nickel; In methanol; ethanol; dichloromethane; water; benzene;
DOI:10.1021/jm00157a012