methyl (S)-N²-benzyloxycarbonyl-N⁴,N⁶-bis-tert-butoxycarbonyl-4-azalysinate

Base Information

Chemical Name:methyl (S)-N²-benzyloxycarbonyl-N⁴,N⁶-bis-tert-butoxycarbonyl-4-azalysinate
CAS No.:241812-15-7
Molecular Formula:C₂₄H₃₇N₃O₈
Molecular Weight:495.573
Hs Code.:

methyl (S)-N<sup>2</sup>-benzyloxycarbonyl-N<sup>4</sup>,N<sup>6</sup>-bis-tert-butoxycarbonyl-4-azalysinate

Synonyms:methyl (S)-N²-benzyloxycarbonyl-N⁴,N⁶-bis-tert-butoxycarbonyl-4-azalysinate

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Chemical Property of methyl (S)-N²-benzyloxycarbonyl-N⁴,N⁶-bis-tert-butoxycarbonyl-4-azalysinate

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Technology Process of methyl (S)-N²-benzyloxycarbonyl-N⁴,N⁶-bis-tert-butoxycarbonyl-4-azalysinate

There total 10 articles about methyl (S)-N²-benzyloxycarbonyl-N⁴,N⁶-bis-tert-butoxycarbonyl-4-azalysinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 239789-53-8
methyl N²-benzyloxycarbonyl-N⁶-tert-butoxycarbonyl-2(S),6-diamino-4-azahexanoate

: 241812-15-7
methyl (S)-N²-benzyloxycarbonyl-N⁴,N⁶-bis-tert-butoxycarbonyl-4-azalysinate

Guidance literature:: In dichloromethane; at 20 ℃; for 18h;
DOI:10.1021/jo010456e

Reference yield:

: 2304-96-3
N-benzyloxycarbonyl-L-asparagine

: 241812-15-7
methyl (S)-N²-benzyloxycarbonyl-N⁴,N⁶-bis-tert-butoxycarbonyl-4-azalysinate

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / iodosobenzene diacetate / ethyl acetate; acetonitrile; H₂O / 4.5 h / 15 - 20 °C

2: 78 percent / HCl / 5 °C

3: 65 percent / acetic acid; sodium cyanoborohydride / methanol

4: 85 percent / CH₂Cl₂ / 18 h / 20 °C

With hydrogenchloride; [bis(acetoxy)iodo]benzene; sodium cyanoborohydride; acetic acid; In methanol; dichloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1021/jo010456e

Reference yield:

: 89711-08-0
N-(t-butoxycarbonyl)glycinal

: 241812-15-7
methyl (S)-N²-benzyloxycarbonyl-N⁴,N⁶-bis-tert-butoxycarbonyl-4-azalysinate

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / acetic acid; sodium cyanoborohydride / methanol

2: 85 percent / CH₂Cl₂ / 18 h / 20 °C

With sodium cyanoborohydride; acetic acid; In methanol; dichloromethane;
DOI:10.1021/jo010456e