2-[4-(2-aminopyrimidin-5-yl)phenyl]-2,3-dimethyl-N-(pyridin-4-yl)butanamide

Base Information

Chemical Name:2-[4-(2-aminopyrimidin-5-yl)phenyl]-2,3-dimethyl-N-(pyridin-4-yl)butanamide
CAS No.:1382484-88-9
Molecular Formula:C₂₁H₂₃N₅O
Molecular Weight:361.447
Hs Code.:

Synonyms:2-[4-(2-aminopyrimidin-5-yl)phenyl]-2,3-dimethyl-N-(pyridin-4-yl)butanamide

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Chemical Property of 2-[4-(2-aminopyrimidin-5-yl)phenyl]-2,3-dimethyl-N-(pyridin-4-yl)butanamide

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Technology Process of 2-[4-(2-aminopyrimidin-5-yl)phenyl]-2,3-dimethyl-N-(pyridin-4-yl)butanamide

There total 2 articles about 2-[4-(2-aminopyrimidin-5-yl)phenyl]-2,3-dimethyl-N-(pyridin-4-yl)butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 402960-38-7
5-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)pyrimidin-2-ylamine

: 1382486-38-5
C₁₇H₁₉BrN₂O

: 1382484-88-9
2-[4-(2-aminopyrimidin-5-yl)phenyl]-2,3-dimethyl-N-(pyridin-4-yl)butanamide

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 120 ℃; for 0.5h; Microwave irradiation;

Reference yield:

: 504-24-5
4-aminopyridine

: 1382486-65-8
C₁₇H₁₇BrN₄O₂

: 1382484-88-9
2-[4-(2-aminopyrimidin-5-yl)phenyl]-2,3-dimethyl-N-(pyridin-4-yl)butanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine / tetrahydrofuran / 1 h / 120 °C / Microwave irradiation

2: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 0.5 h / 120 °C / Microwave irradiation

With sodium carbonate; 2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; N,N-dimethyl-formamide;